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Volatile organic compounds analysis results, March 20, 2002

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Laboratory report detailing analytical results for volatile organic compounds in sample AE05899 collected on March 20, 2002.

NYC-WTC_000021992–000022075

Folder label: “524 3/20/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\02MAR20\0320R5.D Vial: 3 Acq On : 20 Mar 2002 11:43 am Operator: 201-wb Sample : ref 5 Inst : GC/MS Ins Mise : March 20, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 20 14:14 2002 Quant Results File: HP031802.RES Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Wed Mar 20 14:14:30 2002 Response via : Initial Calibration DataAcq Meth : HP031802

Compound R.T. Qlon Response Cone Unit Qvalue 48) P & M-XYLENE 22.01 106 917834 11.20 ug/L 95 49) 0-XYLENE 22.99 91 1056144 5.59 ug/L 100 50) STYRENE 23.04 104 731907 5.84 ug/L 98 51) 1,1,2,2-TETRACHLOROETHANE 24.06 83 200589 5.81 ug/L 97 53) BROMOFORM 23.90 173 126643 6.28 ug/L 95 54) ISOPROPYLBENZENE 23.70 105 1201033 5.97 ug/L 100 55) 1,2,3-TRICHLOROPROPANE 24.40 110 69958 6.45 ug/L 94 56) N-PROPYLBENZENE 24.59 91 1458893 5.58 ug/L 100 57) BROMOBENZENE 24.82 156 338580 6.40 ug/L 91 58) 1,3,5-TRIMETHYLBENZENE 24.89 105 1064708 5.96 ug/L 99 59) 2-CHLOROTOLUENE 25.06 91 1027054 5.71 ug/L 98 60) 4-CHLOROTOLUENE 25.13 91 904088 5.84 ug/L 100 61) TERT-BUTYLBENZENE 25.69 119 956727 5.87 ug/L 100 62) 1,2,4-TRIMETHYLBENZENE 25.78 105 1097467 5.87 ug/L 100 63) SEC-BUTYLBENZENE 26.15 105 1301953 5.82 ug/L 99 64) P-ISOPROPYLTOLUENE 26.41 119 1072434 6.14 ug/L 100 65) 1,3-DICHLOROBENZENE 26.76 146 617335 6.11 ug/L 98 66) 1,4-DICHLOROBENZENE 26.99 146 617536 5.91 ug/L 97 67) N-BUTYLBENZENE 27.29 91 1061241 5.98 ug/L 99 68) 1,2-DICHLOROBENZENE 27.84 146 530794 6.14 ug/L 99 69) 1,2-DIBROMO-3-CHLOROPROPAN 29.61 157 31991 6.03 ug/L 97 70) 1,2,4-TRICHLOROBENZENE 31.91 180 364338 6.68 ug/L 99 71) HEXACHLOROBUTADIENE 32.21 225 199074 7.06 ug/L 95 72) NAPHTHALENE 32.74 128 421270 6.29 ug/L 98 73) 1,2,3-TRICHLOROBENZENE 33.46 180 306589 7.18 ug/L 95 74) NITROBENZENE 29.83 77 149517 118.73 ug/L 96

(#) = qualifier out of range (m) = manual integration 0320R5.D HP031802.M Thu Mar 21 15:56:01 2002 Page 2

NYC-WTC_000022006

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