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Volatile organic compounds analysis results, March 19, 2002

Machine-extracted title · confidence 95%

Laboratory report detailing analytical results for volatile organic compounds in sample AE06055 collected on March 19, 2002.

NYC-WTC_000021969–000021990

Folder label: “524 3/19/02

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\l\DATA\02marl9\0319R5.D Vial: 11 Acq On : 19 Mar 2002 10:46 am Operator: Sample : ref 5 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Mar 19 11:21 2002 Quant Results File: HP031502.RES Quant Method : C:\HPCHEM\1\METHODS\HP031502.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Last Update : Mon Mar 18 14:36:15 2002 Response via : Initial Calibration DataAcq Meth : HP031502

Compound R.T. Qlon Response Cone Unit Qvalue 33) CIS-1,3-DICHLOROPROPENE 16.50 75 185561 5.35 ug/L 98 34) TOLUENE 17.00 91 371632 5.21 ug/L 100 3 5) TRANS-1,3-DICHLOROPROPENE 17.76 75 197724 5.02 ug/L 99 36) 1,1,2-TRICHLOROETHANE 18.10 97 54492 5.28 ug/L 90 37) TETRACHLOROETHENE 17.80 166 154845 5.36 ug/L 95 38) 1,3-DICHLOROPROPANE 18.68 76 115623 5.33 ug/L 96 39) DIBROMOCHLOROMETHANE 18.49 129 127970 5.11 ug/L 97 40) 1,2-DIBROMOETHANE 19.04 107 63339 5.03 ug/L 100 41) CHLOROBENZENE 20.06 112 272271 4.99 ug/L 98 42) 1,1,1,2-TETRACHLOROETHANE 20.16 131 152694 5.03 ug/L 100 43) 2-HEXANONE 17.66 43 244553 — 26.38 ug/L 98 44) ETHYLBENZENE 21.23 91 525109 4.74 ug/L 99 45) P & M-XYLENE 20.33 106 368744 9.75 ug/L 100 46) O-XYLENE 20.33 91 1066622 4.86 ug/L 100 47) STYRENE 21.33 104 264547 4.77 ug/L 98 48) 1,1,2,2-TETRACHLOROETHANE 22.83 83 52609 4.62 ug/L 78 50) BROMOFORM 21.45 173 64623 6.11 ug/L 96 51) ISOPROPYLBENZENE 21.85 105 628486 5.46 ug/L 98 53) 1,2,3-TRICHLOROPROPANE 23.19 110 27320 4.84 ug/L 85 54) N-PROPYLBENZENE 23.12 91 616387 5.38 ug/L 95 55) BROMOBENZENE 22.78 156 143216 5.75 ug/L 95 56) 1,3,5-TRIMETHYLBENZENE 23.94 105 616168 5.43 ug/L 99 57) 2-CHLOROTOLUENE 23.12 91 616387 5.38 ug/L 98 58) 4-CHLOROTOLUENE 23.46 91 550141 5.33 ug/L 96 59) TERT-BUTYLBENZENE 23.80 134 113436 5.65 ug/L 91 60) 1,2,4-TRIMETHYLBENZENE 23.09 105 594971 5.42 ug/L 97 61) SEC-BUTYLBENZENE 24.18 105 702530 5.16 ug/L 99 62) P-ISOPROPYLTOLUENE 24.45 119 646437 4.93 ug/L 99 63) 1,3-DICHLOROBENZENE 24.74 146 288079 5.04 ug/L 95 64) 1,4-DICHLOROBENZENE 24.92 146 296384 5.22 ug/L 97 65) N-BUTYLBENZENE 25.37 91 631258 4.82 ug/L 96 66) 1,2-DICHLOROBENZENE 25.86 146 248824 5.08 ug/L 99 67) 1,2-DIBROMO-3-CHLOROPROPAN 27.59 157 12351 3.96 ug/L 89 68) NITROBENZENE 28.87 77 117678 (7873 ug/L 83 69) 1,2,4-TRICHLOROBENZENE 29.09 180 202984 4.65 ug/L 97 70) HEXACHLOROBUTADIENE 28.95 225 159845 4.84 ug/L 96 71) NAPHTHALENE 29.84 128 205140 4.82 ug/L 98 72) 1,2,3-TRICHLOROBENZENE 30.26 180 168916 4.79 ug/L 98

(#) = qualifier out of range (m) = manual integration 0319R5.D HP031502.M Tue Mar 19 11:21:14 2002 Page 2

NYC-WTC_000021979

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