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Volatile organic compounds blank results, Mar 8 2002

Machine-extracted title · confidence 95%

Laboratory analysis results for volatile organic compounds blank sample AE05178 dated March 8, 2002.

NYC-WTC_000021328–000021450

Folder label: “524 3/8/02 - 3/11/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\02MAR08\5179.D Vial: 16 Acg On 8 Mar 2002 9:57 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 2 Acetonitrile, dichloro- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 17.20 0.03 ug/L 20889 1,4-DIFLUOROBENZENE 15.05 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Thietane 74 C3H6S 000287-27-4 4 3 o-Methylisourea hydrogen sulfate 74 C2H6N2O 029427-58-5 3 4 Propanoic acid 74 C3H602 ______ 000079-09-4 2 Abundance Scan 777 (17.197 min): 5179.D (-) m/z 73.95 100.00% 74 8000

6000 82

4000 16.80 17.00 17.20 17.40 17.60 47 m/z 82.00 55.25% ■‘‘i ‘‘ “ I‘ ' i “ “ i • ■ ■' i ■ ■" i “ ■ ‘ i ‘ “ i' “ ‘ i ■ ‘") ■ ■ ■ ■ i “ ‘ 1 l ■ mmpm m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63810: Acetonitrile, dichloro- 74 35

5000 82 16.80 17.00 17.20 17.40 17.60 38 47 m/z 83.90 35.24%

86 " ‘I “ ''I''" I' ‘11 TT A ooponodyonasjack T ‘" 11 i ■■' ■ i' ■ ‘ ■ i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62560: Thietane 46

16.80 17.00 17.20 17.40 17.60 74 m/z 76.00 32.28% 5000

27 „ 41

m/z-> ,1 38 TTIgp .......59........ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 i ■ ■ ■ ■ i■"'I■" ■ i'' “ i

Abundance #309: o-Methylisourea hydrogen sulfate 44 16.80 17.00 17.20 17.40 17.60 m/z 46.95 31.75%

5000

58 74 >> > J > > > > । >. > > t. > > >| < >. >p I47 il. 1।11111 .1II|। j। 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 16.80 17.00 17.20 17.40 17.60

5179.D HP022702.M Sun Mar 10 13:17:54 2002 Page 2

NYC-WTC_000021397

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NYC-WTC_000021397Source: NYC Law Department, mirrored locally

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