Volatile organic compounds blank results, Mar 8 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02mar11\5177D.D Vial: 5 Acg On : 11 Mar 2002 4:25 pm Operator: 201-wb Sample : nyc dup Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 2 Acetonitrile, dichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

17.16 0.07 ug/L 40916 1,4-DIFLUOROBENZENE 15.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 40 2 Ethenyl t-butyl sulfoxide 132 C6H120S 000000-00-0 4 3 N-Nitrosodimethylamine 74 C2H6N20 000062-75-9 3 4 Ether 74 C4H10O _______ 000060-29-7 3 Abundance Scan 775 (17.162 mln): 5177D.D (-) m/z 73.95 100.00% 74

82 5000 47 • i • > • ■ i ■ Tr 16.80 17.00 17.20 17.40 . | .1 m/z 82.00 57.29% 11 ' ‘ i ‘'1 ‘ i1 “ ' i ■"' i “ ■ i “ “ i m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #63810: Acetonitrile, dichloro- 74

5000 35

47 82 I 16.80 17.00 17.20 17.40 m/z 46.95 39.74%

— ■ i' ■ ■ ■ i • TI TTp-TT-rp-r-r-rp-T i ■•1■i■■1■i■■■■i■■‘ ‘ i ■ • ■' i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5746: Ethenyl t-butyl sulfoxide 41 57 16.80 17.00 17.20 17.40 5000 m/z 76.00 35.51% 27 76

m/z-> . . ao—f*. ’1’1 84 L H i “ ' ■ i ■ ■ ■ ‘ i “ “ i ■ •1 • 132 10 20 30 40 50 60 70 80 90 100 110 120 130 i' ‘ ■ i

Abundance #62544: N-Nitrosodimethylamine 42 74 16.80 17.00 17.20 17.40 m/z 84.00 34.26%

5000 15 30

— 11 59 1 ‘1 “ ■ ■ i' “ i' “ ‘ i “ ■ ‘ i ■ ‘ " i ■ ■ “ i ‘ ■ i' ■ " I ■ i ■ ■ • • i ■ '' ‘ i ‘ ‘ ■ i ■ • ■ ‘ i ' m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 16.80 17.00 17.20 17.40

5177D.D HP022702.M Mon Mar 11 17:05:01 2002 Page 2

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