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← Document results/DEP Box 17/524 3/7/02 - 3/8/02
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Volatile organic compounds results, Mar 7 2002

Machine-extracted title · confidence 95%

Laboratory analysis results for volatile organic compounds sample AE05164 dated March 7, 2002.

NYC-WTC_000021152–000021326

Folder label: “524 3/7/02 - 3/8/02

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Scanned page image, NYC-WTC_000021264
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NYC 9/11 Public Portal Document LLOIdLY DEdL CI LOHpVUrU RCPOL L

Data File C:\HPCHEM\l\DATA\02mar07\5171.D Vial: 20 Acq On 8 Mar 2002 1:10 am Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Oxepanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 15.72 0.04 ug/L 26892 1,4-DIFLUOROBENZENE 15.05 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Oxepanone 114 C6H10O2 000502-44-3 3 2 Butane, 2-(ethenyloxy)-2-methyl- 114 C7H140 029281-39-8 3 3 2H-Pyran-2-one, tetrahydro-4-methyl 114 C6H10O2 001121-84-2 3 4 4-Heptanone 114 C7H140 ________ 000123-19-3 3 Abundance Scan 690 (15.716 min): 5171.D (-) m/z 114.15 100.00%| 1 4

5000 63 A................ 88 15.40 15.60 15.80 16.00 ______________ 50 57 1 m/z 63.05 29.11% ■ i ■ 1 1 1 I • ■ ■ ' i ' ‘ ‘ ‘ i ■ ■ ■ i • 1 ■ i ■ ■ • 1 i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64123:2-Oxepanone 42 55

5000 15.40 15.60 15.80 16.00 27 84 m/z 88.00 26.00? 70 114

' i ■ ‘ ■ i ■ ■ 1 ' i • * । • TIit p-r-r-r-r-p-r-TT-p- m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #3032: Butane, 2-(ethenyloxy)-2-methyl- 43 TT-p-TT-r-p- ‘ ' I ' ‘ ‘ ‘ I ' ‘ ‘ I 15.40 15.60 15.80 16.00 5000 m/z 57.05 19.75%

55 71 85 114' 27 L TH ■ i ■ ' ' ' i ' T-p-TT-T-pr + 1 T-pm-r-p 99 | m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #2880:2H-Pyran-2-one, tetrahydro-4-methyl- 42 55 15.40 15.60 15.80 16.00 m/z 50.05 18.31%

5000

70 114

• i ■1 • ■ । ■ ■ ■ ■ i —4 84 ■ ■ i'1 • ■ i ■ • ■ ■ i • ■ ■ ■ i ■ m/z~> 20 30 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00

5171.D HP022702.M Fri Mar 08 01:49:41 2002 Page 1

NYC-WTC_000021264

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NYC-WTC_000021264Source: NYC Law Department, mirrored locally

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