Volatile organic compounds results, Mar 4 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02MAR04\04516F.D Vial: 32 Acq On 5 Mar 2002 8:33 am Operator: 201-wb Sample nyc fb Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Oxepanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.72 0.03 ug/L 21294 1,4-DIFLUOROBENZENE 15.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Oxepanone 114 C6H10O2 000502-44-3 3 2 2H-Pyran-2-one, tetrahydro-4-methyl 114 C6H10O2 001121-84-2 3 3 Butane, 2-(ethenyloxy) -2-methyl- 114 C7H140 029281-39-8 3 4 4-Heptanone 114 C7H140 ________ 000123-19-3 3 Abundance Scan 689 (15,715 min): 04516F.D (-) m/z 114.05 100.00% 1 4

5000

57 63 88 1.. ..... 15.40 15.60 15.80 16.00 44 | m/z 62.95 29.53% ’I’ ■ i ■ ■ ■ ■ i ' ■ ■ ■ i ' ■ ■ ■ i ' ' ' ' i ' ' ' ‘ i ■

m/z--> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64123:2-Oxepanone 42 55

5000 15.40 15.60 15.80 16.00 27 84 m/z 88.10 28.25% 70 114 T-p-r-n-p-r-n-p ■ ■ i ■ ■ ■ i ■ ‘ T-p-r-T-TT-p-T-TT-p- m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #2880:2H-Pyran-2-one, tetrahydro-4-methyl- 42 55

■ ' i ■ ‘ ' i ■ TT-p-r-r-r-p-n-r-j 15.40 15.60 15.80 16.00 5000 m/z 57.05 22.39%

70 114 T-p-n-r-pr-r-n-r —4 84 ‘ ‘ i ' 1 ’ ■ i ■ ■ ■ ■ i ■ ‘ ■ i •

m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #3032: Butane, 2-(ethenyloxy)-2-methyl- 43 15.40 15.60 15.80 16.00 m/z 44.05 8.92%

5000 MMwMW 55 71 85

m/z--> ... 27 1 । । • • ■ ■ । > PIT 20 30 40 ■ i

50 •...

60 ■ ■

TH • i • »■ ■ i ■ < • • i • > 70 80 90 100 110 99 l 120 15.40 15.60 15.80 16.00

04516F.D HP022702.M Tue Mar 05 11:34:39 2002 Page 2

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