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VOC analysis results, sample AE03944, Feb 20 2002

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Laboratory results for volatile organic compounds in sample AE03944 analyzed on February 20, 2002.

NYC-WTC_000020143–000020240

Folder label: “524 2/20/02

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Scanned page image, NYC-WTC_000020189
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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02feb20\03946.D Vial: 12 Acq On : 20 Feb 2002 5:39 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 20, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 20 18:17 2002 Quant Results File: HP021702.RES Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Tue Feb 19 16:16:43 2002 Response via : Initial Calibration DataAcq Meth : HP021702

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.14 114 1918245 5.00 ug/L 0.02 24) CHLOROBENZENE-D5 21.79 117 1807380 5.00 ug/L 0.03 52) 1,4-DICHLOROBENZENE-D4 26.99 152 795940 5.00 ug/L 0.04 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.39 65 653573 4.48 ug/L 0.04 Spiked Amount 5.000 Recovery = 89.60% 3) 4-BROMOFLUOROBENZENE 24.38 174 586900 4.07 ug/L 0.03 Spiked Amount 5.000 Recovery = 81.40% 25) TOLUENE-D8 18.49 98 2332474 5.20 ug/L 0.02 Spiked Amount 5.000 Recovery = 104.00% Target Compounds Qvalue 9) TRICHLOROFLUOROMETHANE 7.87 101 10231 "6. 17 ug/L 95 10) Isopropyl Alcohol 7.85 45 55709 42.43 ug/L 82 12) ACETONE 8.29 43 67675 - 5.13 ug/L 91 14) METHYLENE CHLORIDE 9.65 49 92322 . -0.83 ug/L 95 15) METHYL TERT BUTYL ETHER 9.96 73 19843 •0.16 ug/L 85 18) 2-BUTANONE (MEK) 12.05 43 31574 1.03-ug/L 94 21) CHLOROFORM // 12.86 83 2548612 18.20 ug/L 99 33) BROMODICHLOROMETHANE 16.82 83 541588 5.74 ug/L 99 37) TOLUENE 18.68 91 48980 -018 ug#E — 94 42) DIBROMOCHLOROMETHANE , 6 0 20.55 129 36151 0.68 ug/L 98

(#) = qualifier out of range (m) = manual integration 03946.D HP021702.M Wed Feb 20 18:18:07 2002 Page 1

NYC-WTC_000020189

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NYC-WTC_000020189Source: NYC Law Department, mirrored locally

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