VOC analysis results, sample AE03944, Feb 20 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02feb20\03959B.D Vial: 8 Acq On : 20 Feb 2002 2:46 pm Operator: 201-wb Sample : nyc re-inj Inst : GC/MS Ins Mise : February 20, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 20 15:24 2002 Quant Results File: HP021702.RES Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Tue Feb 19 16:16:43 2002 Response via : Initial Calibration DataAcq Meth : HP021702

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.12 114 2199304 5.00 ug/L 0.00 24) CHLOROBENZENE-D5 21.78 117 2099912 5.00 ug/L 0.01 52) 1,4-DICHLOROBENZENE-D4 26.95 152 964940 5.00 ug/L 0.00 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 720478 4.30 ug/L 0.00 Spiked Amount 5.000 Recovery = 86.00% 3) 4-BROMOFLUOROBENZENE 24.36 174 709061 4.29 ug/L 0.00 Spiked Amount 5.000 Recovery = 85.80% 25) TOLUENE-D8 18.47 98 2691205 5.17 ug/L 0.00 Spiked Amount Target Compounds 5.000 Recovery = 103.40% tp D(" Qvalue 4

7) BROMOMETHANE 6.63 94 5096 0.14ug/L 97 9) TRICHLOROFLUOROMETHANE 7.30 101 8200 0.12jug/L 85 12) ACETONE 8.28 43 48425 3.20 ug/L 92 14) METHYLENE CHLORIDE 9.64 49 99660 —0.8 ug7L 97 15) METHYL TERT BUTYL ETHER 9.94 73 14540 0.10 ug/L 90 18) 2-BUTANONE (MEK) 12.04 43 28001 000 ug/L 96 21) CHLOROFORM 21 12.84 83 3489913 21.74 ug/L 98 33) BROMODICHLOROMETHANE 2 S 16.80 83 802274 7.31 ug/L 100 37) TOLUENE 18.66 91 21165 0 407 ug/E 94 42) DIBROMOCHLOROMETHANE t 20.53 129 58333 0.94 ug/L 92 (, 72) NAPHTHALENE 32.83 128 45060 0.41 ug/L 97 I / 73) 1,2,3-TRICHLOROBENZENE 33.52 180 12653 0.19 ug/L 92

(#) = qualifier out of range (m) = manual integration 03959B.D HP021702.M Wed Feb 20 15:25:04 2002 Page 1

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