VOC analysis results, sample AE03015, Feb 15 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB15\03014.D Vial: 11 Acq On : 15 Feb 2002 4:34 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 Ethanedial, dioxime Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 15.77 0.04 ug/L 21832 1,4-DIFLUOROBENZENE 15.11 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanedial, dioxime 88 C2H4N202! 000557-30-2 4 2 2,3-Dioxabicyclo [2.2.2]octane 114 C6H10O2 000000-00-0 4 3 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H204 002892-51-5 4 4 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2!006843-45-4 3 Abundance Scan 683 (15.773 min): 03014.D (-) m/z 114.15 100.00% 1 4

5000

63 88 15.40 15.60 15.80 16.00 | .............. 40........... .............. i ■ ‘ ' l' ‘ ■ 11 ■ ’ I** m/z 63.05 28.90% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #783: Ethanedial, dioxime 44 16 27 88 70 5000 ' I ■ ■ ■ ■ i ■ ' ■ ■ i ■' ■ ■ i ‘ ■ 1 ■ i' 15.40 15.60 15.80 16.00 53 m/z 88.00 21.58%

m/z-> 10 ■ i ■' ■ i ■ • 20 J 30 4 40 50 60 70 80 90 100 110 120 ■ ■ i1 ■ j_____________________ i ■ ■'' i' ■ ■' i ■ ■ ■ ■ i ■'

Abundance #2867:2,3-Dioxabicycto[2.2.2]octane 29 ' I' ■ ■ ■ i ■' I '111 111 1 ' I ' 15.40 15.60 15.80 16.00 5000 81 m/z 40.00 8.16% 57

AWAMAA W 114 44 NV 67 .1 ।.. J. ।... . ... । . j j 11111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #64087: 3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 29 TT 58 15.40 15.60 15.80 16.00

5000 114

.......... 141..... ■ i ■ ■ ■ ■ i ■'1 ■ i1 ’+-14-4*1** 68 86 I ' ' ' ‘ I • ‘ ‘ ‘ I 1 11 ‘ T-^’1 1 1 1 1 1 | ' m/z--> 10 20 30 40 50 60 70 80 90 100 110 120

03014.D HP021702.M Mon Feb 25 13:03:09 2002 Page 1

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