VOC analysis results, sample AE03015, Feb 15 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB15\03380.D Vial: 26 Acq On : 16 Feb 2002 4:42 am Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Urea, N,N-dimethyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 15.79 0.04 ug/L 33460 1,4-DIFLUOROBENZENE 15.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Urea, N,N-dimethyl- 88 C3H8N20 000598-94-7 5 2 2,3-Dioxabicyclo[2.2.2]octane 114 C6H10O2 000000-00-0 4 3 1,4-Butanediamine 88 C4H12N2 000110-60-1 3 4 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O21_______ 006843-45-4 3 Abundance Scan 684 (15.792 min): 03380.D (-) m/z 114.15 100.00%| 1 4

5000 63

................................................. .................. 88 w....... . 15.40 15.60 15.80 16.00 16.20 ■ ■ i ‘ ■ i1 • ■ ■ i' ■ ■1111'' 111'' I'111 f1''1111 i1'1111 ‘ ‘ i1 m/z 63.05 25.67% • ■ i • ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62896: Urea, N,N-dimethyl- 44

5000 88 i ■ ■ ■ ■ i '' T ' ' I ‘ ‘ ' I ' ‘ 15.40 15.60 15.80 16.00 16.20 m/z 88.10 21.84%

m/z-> Abundance 15 — 30

10 20 + 56 72 30 TIITTIWTIITTTTT 40 50 60 70 80 90 100 110 120 #2867:2,3-Dioxabicyclo[2.2.2]octane i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■

29 I ‘ ■ I ' ‘ ■ ' I • ■ • ■ l < • 15.40 15.60 15.80 16.00 16.20 5000 81 m/z 57.05 12.619 57 114 44 67

m/z-> 10 • • i • ■ > ■ i ■ ‘ 20 HPPmm 30 40 50 60 70 80 90 100 110 120 Abundance #828: 1,4-Butanediamine 30 15.40 15.60 15.80 16.00 16.20 m/z 43.95 5.71 AWyAMW 5000 43

59 . ............. . 70 88 • i • • ■ > i < ■ ■ ' I’’ ■ ■ ■ i ■ ■ ■ 1 i ■ 1 ' ‘ 1 1 ■ 1 ■ i ■ ■ ■ ■ i ■ ■ m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00 16.20

03380.D HP021302.M Mon Feb 18 15:28:47 2002 Page 1

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