VOC analysis results, sample AE03015, Feb 15 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB15\03250.D Vial: 24 Acq On : 16 Feb 2002 3:08 am Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Urea, N,N-dimethyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

15.79 0.04 ug/L 36072 1,4-DIFLUOROBENZENE 15.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Urea, N,N-dimethyl- 88 C3H8N20 000598-94-7 4 2 2,3-Dioxabicyclo [2.2.2]octane 114 C6H10O2 000000-00-0 4 3 1,4-Butanediamine 88 C4H12N2 000110-60-1 3 4 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N202 006843-45-4 3 Abundance Scan 684 (15.791 min): 03250.D (-) m/z 114.05 100.00% 1 4

5000

50 63 88 w... 15.40 15.60 15.80 16.00 16.20

m/z-> 10 1.... 40111 • < I • > m/z 63.05 20 30 40 50 60 70 80 90 100 110 120 ■ i ■ ■ ‘' i ■ • ■ ■ i ‘ ■ i ■ ■ • ‘ i' ■ ■ ■ 11 23.05%

Abundance #62896: Urea, N,N-dimethyl- 44

5000 88 11 ■ ‘ • i ■ ■ ‘ ■ i ■ ' i' ■ ■ ■ i ‘' 15.40 15.60 15.80 16.00 16.20 m/z 88.00 19.94% —15 A

m/z-> 10 20 30

30 +L 40 56 72 11111 ’' I ■ ■ ■ ■ i' ■ ■ ■ i ■ ‘ 50 60 90 100 110 120 70 80 i ■ ■ ■ ■ i ■' ■ ■ P ' ■ ■ i ■ ■

Abundance #2867:2,3-Dloxabicyclo[2.2.2]octane 29 i ‘ ■ i ■ ■ I1 11 1 I' 11111' 15.40 15.60 15.80 16.00 16.20 5000 81 m/z 57.05 13.06% 57 114 44 67 ••i • > ’I8 ■' i ■ • • ‘ i ■ ■ ■' i' • * [ *1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #828:1,4-Butanediamine 33 i ■ ■1 ■ i' ■ i1 ■1 ■ i ■ ■ ‘ ■ i' ■ 15.40 15.60 15.80 16.00 16.20 m/z 50.05 10.98%

5000 43

n/z--> ••। > > •■ । 10 20 ■ L 1

30 40 .

50 59

60 70 88 ■ ■ I-' ■ ■ ■ i ■ ■ ■ 1 i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ' ■ i ■ ' 70 80 90 100 110 120 15.40 15.60 15.80 16.00 16.20

03250.D HP021302.M Mon Feb 18 15:26:42 2002 Page 1

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