NYC 9/11 Public Portal Document
Data File C: \HPCHEM\1\DATA\02f eb08\2581FB. D Vial: 16
Acq On 9 Feb 2002 4:44 am Operator: 201-wb -do
is
Sample nyc 524 filed bl Inst : —im
GC/MS Ins-il
Mise Multiplr: 1.00 life
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\HP020502.M (RTE Integrator) of
Title : VOCs BY EPA METHOD 524 -
-fi
Library : C:\DATABASE\NBS75K.L ..a
********************************************************************* —
Peak Number 4 2,4-Imidazolidinedione, 3-meth Concentration Rank 4
-
I MB
R.T. EstConc Area Relative to ISTD R.T.
-ie
15.76 0.04 ug/L 50898 1,4 -DIFLUOROBENZENE 15.10
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2 006843-45-4 3
2 1-(Propenylthio)prop-1-ene 114 C6H10S 000000-00-0 3
3 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H204 002892-51-5 2
4 Ethyl diazoacetate 114 C4H6N2O2_ _____ 000623-73-4 2
Abundance Scan 682 (15.757 min): 2581 FB.D (-) m/z 114.15 100.00%
1 4
-storm
ii a
5000 -
63 88
39 44 50 57 94 15.40 15.60 15.80 16.00
n/z->
......
20
11 1 ...........
I ' ' ' ' I ’ ’ ’ ' I ' 1 ‘ 1 I ' ' • ' I ‘
30 40 50 60 70
' I ' ' ’ * I ' ‘
80
AX 90
i ■ ■ ■ ' i '
100 110 ' 120 '
m/z 63.15 24.31%
-f
Abundance #64088:2,4-lmidazolidinedione, 3-methyl- a
1 4
-
life
58
5000
15.40 15.60 15.80 16.00 " ‘ '
86 m/ z 88.10 23.21% -lt
42 71
1**’’I***11** ■ ।' । ■'' ■ । ■ • ‘ I ‘ 1
n/z—> 20 30 40 50 60 70 80 90 100 110 120
Abundance #2940: 1-(Propenylthio)prop-1-ene
41 1 4
99
' ■ i ' ' ' ■ i 1 ■ 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■
15.40 15,60 15.80 16.00
5000 m/z57.05 10.99%
59 85 -untni
47 I m
i ‘ • i ■ ■ ■ ■ i‘ ■ 4 i ‘ ' • i ■ ■ i • • ■ ■ i ‘ ■ I ■ ‘ ■ i ■
' 120
mfe-> 20 30 40 50 60 80 90 100 110 -
Abundance #64087: 3-Cyclobutene-1,2-dione, 3,4-dihydroxy- ■ ■ । ■
-
d.
29 58 15.40 15.60 15.80 16.00
m/ Z 94.20 10.89%
-
5000 114
—a
nm
n/z—>
. I
I ‘
20 30
——
41
' 'I' ‘
40 50 60
68
70 80
86
90
144*1++*1**I--‘I‘‘‘I*
100 110
' ' I ' '
120 15.40 15.60 15.80 16.00
2581FB.D HP020502.M Sat Feb 09 05:24:40 2002 Page 4
NYC-WTC_000019719
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