SB1524 volatile analysis results, sample AE01938, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02FEB04\01942.D Vial: 12 Acq On : 4 Feb 2002 6:26 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2H-Pyran-2-one, tetrahydro-4-m Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

15.81 0.04 ug/L 33806 1,4-DIFLUOROBENZENE 15.15

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2H-Pyran-2-one, tetrahydro-4-methyl 114 C6H10O2 001121-84-2 3 2 4-Heptanone 114 C7H140 000123-19-3 3 3 3-Hexanone, 2-methyl- 114 C7H14O 007379-12-6 3 4 1-(Propenylthio)prop-1-ene 114 C6H10S 000000-00-0 3 Abundance Scan 685 (15.809 min): 01942.D (-) m/z 114.15 100.00% 1* 4

5000 63 88 ‘ ■ i ■ ■ 57 15.40 15,60 15.80 16.00 16.20 4 ■ i ' ‘ ■ i ■ ■ ■ ' i ' ■ ■ ■ i ' ' ' ' i ‘ ‘ ' i ■ ' ■ ■ i ' ' 11 ■ ■ ■ 11 ■' ' । • • ' ■ । ■ 1 m/z 63.05 N 25.55% niz-> 20 30 40 50 60 90 70 100 80 110 120 Abundance #2880:2H-Pyran-2-one, tetrahydro-4-methyl- 42 55

5000 15.40 15.60 15.80 16.00 16.20 70 114 m/z 88.10 25.05%

miz—> 20 30 40 —4 50 ■ i ■ ■ 60 .J70..80 44..... 90 100 -- 110 120 Abundance #64152: 4-Heptanone 43 71 15.40 15.60 15.80 16.00 16.20 5000 m/z 57.15 15.65% 27

114 58 99 | miz-> 20 .. ... 30 JI 40 1 •'■’l 1 50 60 70 80 90 100 110 120 Abundance #64191:3-Hexanone, 2-methyl- i ■ ■ ■ ' i 1 ■ 43 15.40 15.60 15.80 16.00 16.20 m/z 44.05 5.27% 5000 71 AA 27 114 55 miz—> ■ i • ■ ■ ■ i ■ ' 20 30 ■ ‘ r 40 1 ■ ' i ' ' ■■ ■ ! ’ ' ■ ' l 50 60 70 ..80 86,1, 90 99..... hI..,.. 100 110 120 15.40 15.60 15.80 16.00 16.20

01942.D HP013102.M Tue Feb 05 09:47:51 2002 Page 3

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