SB1524 volatile analysis results, sample AE01938, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02FEB04\01938.D Vial: 9 Acq On 4 Feb 2002 4:16 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Guanidine, methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

9.98 0.03 ug/L 23131 1,4-DIFLUOROBENZENE 15.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Guanidine, methyl- 73 C2H7N3 000471-29-4 3 2 1-Propanamine, 2-methyl- 73 C4H11N 000078-81-9 3 3 1 - But anamine 73 C4H11N 000109-73-9 3 4 2-Butanamine, 73 C4H11N 033966-50-6 3 Abundance Scan 349 (9.978 min): 01938.D (-) m/z 73.05 100.00% 73

5000 43 57

9.60 9.80 10.00 10.20 10.40 40 m/z 43.05 47.05% 111 " ' I " " 11 “ i'1' ■ i''' ■ i • " ■ i'1' ■ i1' ■ ■ i' ■ ■' i ‘' ■ ■ i ■ ■ ■ ■ i ■ ■ ■' i'' miz-> Abundance 5 10 15 20 25 30 35 40 33 45 50 55 #285: Guanidine, methyl- 60 65 70 75 80 N 43 73

5000 ■ i ' 1 ■ ■ i ' 1 9.60 9.80 10.00 10.20 10.40 57 m/z 41.15 43.58% 17

m/z-> 5 —l— 10 15 20 - 27 25 i ■ ■111 ■ ... . 30 35 40 45 50 55 60 65 70 11 ■ ■' ■ i' ■ 75 80 A

Abundance #62540:1-Propanamine, 2-methyl- 30 9.60 9.80 10.00 10.20 10.40 5000 m/ z 57.05 36.59%

27 43 46 5558 73 ■ i ■ ■ ■ ■ i11.' i1. ■. i' ■ “ 11 ■1 ■ r ■ ■ ■ i ■ ■ ■ ■ i' ■ I ■ i ■ ■ " .' ■ " ! " '' I''1'.'1" I'1 " ' mlz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #299:1-Butanamine ■ i ■ • ■ ■ । 1 ■ । । 1 * * । > ■ ■ ■ । ■ ■ 33 9.60 9.80 10.00 10.20 10.40 m/z 43.95 4.72% 5000 AWwww 73 27 41 44 55 iz—> ’' I' ‘' ■ I " " I' - " I ‘1" 1''' i''''.11'11 ■ " ' i'' ‘. i.''' i " ' ‘ i ‘ 5 10 15 20 25 30 35 40 45 50 55 60 65 791..... 70 75 80 9.60 9.80 10.00 10.20 10.40

01938.D HP013102.M Tue Feb 05 09:39:51 2002 Page 1

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