SB1524 volatile analysis results, sample AE01938, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\02FEB04\01936.D Vial: 7 Acq On 4 Feb 2002 2:17 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2,4-Imidazolidinedione, 3-meth Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.83 0.04 ug/L 35183 1,4-DIFLUOROBENZENE 15.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2 006843-45-4 3 2 1-(Propenylthio)prop-1-ene 114 C6H10S 000000-00-0 3 3 3-Cyclobutene-1,2-dione, 3,4-dihydr 114 C4H204 002892-51-5 2 4 Ethyl diazoacetate 114 C4H6N2O2 000623-73-4 2 Abundance Scan 686 (15.827 min): 01936.D (-) m/z 114.05 100.00% 1 4

5000 ............... ....... 63 88 40 57 15.40 15.60 15.80 16.00 16.20 IIIIII110a0GG m/ Z 63.05 25.79% m/z—> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64088:2,4-lmidazolidinedione, 3-methyl- 114

58 5000- 15.40 15.60 15.80 16.00 16.20 86 m/z 88.00 24.09% A 42 71 ■ i ■ 1 1 ri ■ ■ ■ 1 i ■ ■ ■ ■ i ' ■ m/z—> 20 30 40 50 60 70 80 90 100 110 120 Abundance #2940:1-(Propenylthio)prop-1-ene 41 1 4 99 15.40 15.60 15.80 16.00 16.20 5000- m/z 40.05 17.05% N 59 73 85 A Nl 47 I ' ' ' ' I ' ' ' ' I T •I ' ■ i । ■ i ■ ■ ■ ■ i ■ 'I..... ' 1 i 1 ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64087: 3-Cyclobutene-1,2-dione, 3,4-dihydroxy- i ■ ' ' ' i • ' ■ 1 i • ' ■ ' i ■ 1 • i • ■ 29 58 15.40 15.60 15.80 16.00 16.20 m/ Z 56.95 14.89%

5000 114

•I... 41... 1 1 1 1 I' 1 ' 1 1 1 1 1 ' 1 1 1 68 86 I 1 ' ‘ 1 1 1 ' 1 1 1 1 ‘ 1 * I 1 1 ' ' I ' 1 * ‘ I ' i ■ ■ ' ■ i ■ ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00 16.20

01936.D HP013102.M Wed Feb 13 10:37:26 2002 Page 3

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