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GC/MS calibration data for sample 28323, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018519–000018545

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018522
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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data Pile : C:\HPCHEM\l\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS. 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF • Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.141 222 228 239 rBV3 41116 173076 1.22% 0.158% 2 7.618 276 280 297 rBV 221251 742137 5.25% 0.677% 3 11.125 657 662 677 rBV 940839 2344258 16.58% 2.138% 4 11.676 717 722 734 rBV 3066879 7616619 53.86% 6.945% 5 12.511 803 813 817 rBV2 89897 303445 2.15% 0.277%

6 12.658 824 829 839 rVB 90138 221404 1.57% 0.202% 7 12.952 855 861 870 rVB3 68778 262355 1.86% 0.239% 8 13.870 957 961 965 rW 105012 234816 1.66% 0.214% 9 14.311 998 1009 1016 rBV 3106970 6940956 49.08% 6.329% 10 15.284 1109 1115 1143 rBV 4011055 9881101 69.87% 9.010%'

11 17.450 1343 1351 1361 rBV 4040748 9848309 69.64% 8.980% 12 17.579 1361 1365 1380 rVB5 40369 147960 1.05% 0.135% 13 18.157 1422 1428 1434 rBV 254307 524396 3.71% 0.478% 14 20.278 1652 1659 1668 rBV 3366689 7832945 55.39% 7.142% 15 20.563 1683 1690 1704 rBV 4462504 10490378 74.18% 9.565%

16 20.737 1704 1709 1715 rVB 119765 273389 1.93% 0.249% 17 21.031 1736 1741 1760 rVB 278189 964889 6.82% 0.880% 18 22.793 1926 1933 1947 rBV 2435784 5633347 39.83% 5.137% 19 24.978 2162 2171 2211 rBV3 4170121 14142294 100.00% 12.895% 20 26.888 2373 2379 2389 rBV 1387601 3063215 21.66% 2.793%

21 28.650 2564 2571 2579 rBV 1111678 2499473 17.67% 2.279% 22 30.064 2719 2725 2733 rBV 491369 1078607 7.63% 0.983% 23 30.248 2738 2745 2756 rW 1024657 2358560 16.68% 2.151% 24 31.717 2897 2905 2917 rBV 905213 2211971 15.64% 2.017% 25 33.020 3040 3047 3051 rBV2 2688353 7026230 49.68% 6.407%

26 33.084 3051 3054 3073 rW 966389 2605754 18.43% 2.376% 27 34.370 3186 3194 3210 rBV 654059 1814654 12.83% 1.655% 28 35.572 3316 3325 3346 rBV 425296 1356792 9.59% 1.237%

NYC-WTC_000018522

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NYC-WTC_000018522Source: NYC Law Department, mirrored locally

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