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GC/MS calibration data for sample 30645, Dec 2001

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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018470–000018491

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C: \HPCHEM\ 1 \DATA\DEC2 701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 1 8:41 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenyl amine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.04 178 1834 N.D. 34) Anthracene 25.20 178 709 N.D. 35) Di-n-butylphthalate 27.00 149 78657 0.30 ug/1 36) Fluoranthene 28.75 202 822 N.D. 39) Pyrene 29.40 202 792 N.D. 40) Butylbenzylphthalate 31.50 149 593 N.D. 41) Benzo(a)anthracene 33.03 228 8892 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 5259 N.D. 43) Chrysene 33.03 228 8892 N.D. 45) Di-n-Octylphthalate 35.05 149 566 N.D. 4 6) Benzo(b)fluoranthene 36.10 252 1381 N.D. 47) Benzo(k)fluoranthene 36.10 252 1069 N.D. 48) Benzo(a)pyrene 37.12 252 5579 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30645.D GCMS1126.M Fri Feb 01 08:42:29 2002 Page 2

NYC-WTC_000018471

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NYC-WTC_000018471Source: NYC Law Department, mirrored locally

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