Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
NYC-WTC_000018420–000018435Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : M:\INSTRU~1\209\DATA\DEC2701\LBE.D Vial: 51 Acq On : 30 Dec 2001 8:17 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 31 16:11 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title •: 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 1026494 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3916851 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 1889433 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 2834806m 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1740636 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 967290 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.07 235 112951 3.62 ug/mL 0.00 Spiked Amount 5.000 Recovery = 72.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.22 74 258 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2' -oxybis (1 -Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1179 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.27 165 102 N.D. 25) Diethylphthalate 22.14 149 648 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration LBE.D GCMS1126.M Thu Jan 31 16:12:12 2002 Page 1
NYC-WTC_000018421
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