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GCMS analysis results for sample AD31467, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31467 conducted on February 11, 2002.

NYC-WTC_000018396–000018404

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018401
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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\JAN1602\31467.D Vial: 26 Acq On : 17 Jan 2002 1:03 pm Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.452 258 262 292 rBV 309485 922477 14.20% 2.767% 2 11.501 698 703 728 rBV 2013114 5013561 77.18% 15.036% 3 15.090 1089 1094 1112 rBV 3050007 6359864 97.90% 19.074% 4 20.360 1662 1668 1688 rBV 3116194 6496347 100.00% 19.484% 5 24.776 2142 2149 2161 rBV2 2763426 5959980 91.74% 17.875%

6 29.852 2697 2702 2711 rBV 329314 656253 10.10% 1.968% 7 32.799 3017 3023 3045 rBV2 1919777 4509637 69.42% 13.525% 8 36.866 3459 3466 3481 rBV 1276891 3424557 52.72% 10.271%

Sum of corrected areas: 33342676

31467.D GCMS0103.M Thu Feb 07 12:43:04 2002

NYC-WTC_0000 18401

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NYC-WTC_000018401Source: NYC Law Department, mirrored locally

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