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GCMS analytical comments for sample AD30986, Jan 2002

Machine-extracted title · confidence 100%

Analytical notes regarding GCMS scan results and LCS standard recoveries for sample AD30986.

NYC-WTC_000018287–000018315

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\ JANI 802\30986A.D Vial: 3 Acq On 18 Jan 2002 5:36 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 18 18:24 2002 Quant Results File: GCMS0103.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.85 178 506 N.D. 34) Anthracene 24.97 178 117 N.D. 35) Di-n-butylphthalate 26.79 149 15170 N.D. 3 6) Fluoranthene 28.46 202 784 N.D. 3 9) Pyrene 29.11 202 1253 N.D. 40) Butylbenzylphthalate 31.30 149 2035 N.D. 41) Benzo(a)anthracene 32.88 228 10259 N.D. 42) Bis(2-ethylhexyl)phthalate 33.10 149 13755 N.D. 43) Chrysene 32.88 228 10259 N.D. 45) Di-n-Octylphthalate 34.84 149 3076 N.D. 46) Benzo(b)fluoranthene 35.91 252 12061 N.D. 47) Benzo(k)fluoranthene 35.91 252 9104 N.D. . 48) Benzo(a)pyrene 36.73 252 4061 N.D. 4 9) Indeno(1,2,3- cd)pyrene 40.50 276 3005 N.D. 5 0) Dibenz(a,h)anthracene 40.49 278 1876 N.D. 51) Benzo(g,h,i)perylene 41.49 276 3668 N.D.

(#) = qualifier out of range (m) = manual integration 30986A.D GCMS1126.M Tue Jan 22 10:13:05 2002 Page 2

NYC-WTC_000018289

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NYC-WTC_000018289Source: NYC Law Department, mirrored locally

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