Laboratory report documenting GCMS analysis of sample AD28968 conducted on January 9, 2002.
NYC-WTC_000018026–000018035Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC1201\28968.D Vial: 31 Acq On : 13 Dec 2001 7:15 am Operator: 209 GALOS Sample : gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 13 15:48 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.67 152 1112656 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 4263503 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 2159455 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 3044488 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1972694 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1233779 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 170025 3.86 ug/mL -0.02 Spiked Amount 5.000 Recovery = 77.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.16 74 201 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 13.57 82 185 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.32 128 420 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 20.54 153 235 N.D. 24) 2,4-Dinitrotoluene 21.11 165 292 N.D. 25) Diethylphthalate 22.07 149 746 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 22.87 77 188 N.D.
(#) = qualifier out of range (m) = manual integration 28968.D GCMS1126.M Mon Dec 31 14:51:37 2001 Page 1
NYC-WTC_000018028
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