GCMS analysis results for sample AD30470, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD30470 conducted on January 24, 2002.

NYC-WTC_000017903–000017912

Folder label: “GCMS X 12/14/01 A 12/31/01”

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Data File : C:\HPCHEM\1\DATA\DEC3101\30470.D Vial: 9 Acq On : 31 Dec 2001 6:46 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Decanedioic acid, bis(2-ethylh Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

35.57 2.26 ug/1 301802 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Decanedioic acid, bis(2-ethylhexyl) 426 C26H50O4 000122-62-3 64 2 Propanedioicacid, hexyl-, diethyl 244 C13H2404 005398-10-7 38 3 1-Penten-3-one, 4-methyl- 98 C6H10O 001606-47-9 22 4 1-Decene, 2,4-dimethyl- 168 C12H24 055170-80-4 16 Abundance * Scan 3326 (35.575 min): 30470.D (-) 9m/z 185." 100.00% 185 57

5000 43 71 112 98 T T T T Tit

miz-> 20 4 — ,5.44 +2 4— 40 60 166 19 143 1 > ‘i . , । | 203 4 240 281 297 315 . । .. j . . . . | . . . . । , , . > 1 . . . ■'! . . . 1 । . 80 100 120 140 160 180 200 220 240 260 280 300 320 35.20 35.40 35.60 35.80 36.00 m/z 57.00 74.41% Abundance #55661: Decanedioic acid, bis(2-ethylhexy!) ester ............ ) 1$5

5000 57 —M1r 1 I1 71 35.20 35.40 35.60 35.80 36.00

L 112 98 ; m/z 55.00 51.55% 143 166 203 298 316 T* ‘ • 118 1 ‘ 1 ‘ ‘ ‘ 11 T TT ■ ■ i'' ■ • • i'1 ‘ • i ‘ •1 ■ i1 • • ■ i ■ • • ‘ i' •'11 ■ mz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 Mf 71 Tanuii lnmfm 35.20 35.40 35.60 35.80 36.00 5000 112 m/z 71.10 48.91% 83 42 1,98 114444144**04*8414888/3811*** 199 217 i' ■ ■ ■ i" m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #63186: 1-Penten-3-one, 4-methyl- ■ 11.., ।। z Impre 1 । 55 35.20 35.40 35.60 35.80 36.00 m/z 70.10 47.54% 27 5000

70 i .......................................................... —PIPrt miz-> 20 40 60 80' 100 120' 140 160 180 200 220 240 260 280 366' 320 35.20 35.40 35.60 35.80 36.00

30470.D GCMS1126.M Wed Jan 16 08:22:29 2002 Page 2

NYC-WTC_000017911

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GCMS analysis results for sample AD30472, Jan 2002 · Box DEP Box 16

NYC-WTC_000017931

Laboratory report documenting GCMS analysis of sample AD30472 conducted on January 24, 2002.

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