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GCMS blank analysis results for sample AD30605, Jan 2002

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Laboratory report documenting GCMS blank analysis for volatile organic compounds on sample AD30605 conducted on January 10, 2002.

NYC-WTC_000017542–000017555

Folder label: “GCMS X 12/20/01 A 1/9/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\JAN0 8 02\LBB.D Vial: 18 Acq On 9 Jan 2002 5:55 am Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 9 10:18 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue 30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.87 178 1224 N.D. 3 4) Anthracene 25.03 178 662 N.D. 35) Di-n-butylphthalate 26.84 149 3878 N.D. 36) Fluoranthene 28.51 202 560 N.D. 39) Pyrene 29.17 202 762 N.D. 40) Butylbenzylphthalate 31.33 149 3920 N.D. 41) Benzo(a)anthracene 32.84 228 3816 N.D. 42) Bis(2-ethylhexyl)phthalate 33.13 149 29457 0.37 ug/1 97 43) Chrysene 32.90 228 911 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 4 6) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. . 48) Benzo(a)pyrene 36.91 252 2968 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration LBB.D GCMS0103.M Wed Jan 09 11:45:18 2002 Page 2

NYC-WTC_000017544

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Laboratory report listing quantitative results for numerous organic compounds in a GCMS calibration sample analyzed on January 9, 2002.

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GCMS reference scan results · Box DEP Box 16

NYC-WTC_000017537

Laboratory report listing quantitative results for numerous organic compounds in a GCMS reference scan of sample AD30605 on January 9, 2002.

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