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GCMS analysis log for sample AD31073

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31073 performed on January 18, 2002.

NYC-WTC_000017434–000017458

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document ye Quantitation Report (QT Reviewed) “+ Data File : C:\HPCHEM\1\DATA\JAN0802\31073.D Vial: 10 Acq On : 8 Jan 2002 10:07 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 8 22:56 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Jan 07 10:31:02 2002 Response via : Initial Calibration Datfaaca Meth : GCMSO103 Internal Standards R.T. Qlon Response Conc Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.53 152 784612 20.00 ug/l 0.00 10) Naphthalene-ds 15.12 136 3024943 20.00 ug/l 0.00 17) Acenaphthene-d10 20.39 164 1484713 20.00 ug/l 0.00 29) Phenanthrene-di0 24,80 188 2183746 20.00 ug/1 0.00 38) Chrysene-d12 32.84 240 1377119 20.00 ug/l 0.00 44) Perylene-di2 36.90 264 788793 20.00 ug/l 0.00 System Monitoring Compounds 37) 2,4-DDD 29.88 235 110611 4.41 ug/ml -0.19 Spiked Amount 5.000 Recovery = 88.20% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.11 74 219 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 ° N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 ° N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 ° N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0) N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 ° N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 14.15 93 215 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 ° N.D. 15) Naphthalene 15.19 128 1462 N.D. 16) Hexachlorobutadiene 0.00 225 ° N.D. 18) Hexachlorocyclopentadiene 0.00 237 0) N.D. 19) 2-Chloronaphthalene 18.21 162 192 N.D. 20) Dimethylphthalate 19.80 163 235 N.D. 21) 2,6-Dinitrotoluene 20.12 165 380 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.48 153 258 N.D. 24) 2,4-Dinitrotoluene 20.86 165 1851 N.D. 25) Diethylphthalate 21.92 149 2094 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0) N.D. 27) Fluorene 21.99 166 177 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 31073.D GCMS0103.M Wed Jan 09 11:54:30 2002 Page 1 NYC-WTC_000017436

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NYC-WTC_000017436Source: NYC Law Department, mirrored locally

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