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GCMS analysis results for sample AD30607, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD30607 including DDD surrogates on January 22, 2002.

NYC-WTC_000017171–000017191

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document

Tentatively Identified Compound (LSC) summary

Operator ID: 209 GALOS Date Acquired: 28 Dec 2001 9:15 pm Data File: M:\INSTRU~l\209\DATA\DEC2701\30607.D Name: GC/MS SCAN 12/17 Mise: Method: C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title: 209 625/TCLP calibration table Library Searched: C:\DATABASE\NBS75K.L

TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc

3 - Pentanol , 3 -methyl 7.62 3.0 ug/1 922486 ISTD01 11.67 6215000 20.0 2-Propanone, 1,1,1-t 7.75 0.7 ug/1 221136 ISTD01 11.67 6215000 20.0 Cyclopentasiloxane, 14.31 1.2 ug/1 471111 ISTD02 15.28 7732850 20.0 Cyclohexasiloxane, d 17.45 3.9 ug/1 1524070 ISTD02 15.28 7732850 20.0 3 - Isepropoxy-1,1,1,7 20.28 2.9 ug/1 1205560 ISTD03 20.56 8384120 20.0 Benzoic acid, 4-etho 21.05 0.8 ug/1 343901 ISTD03 20.56 8384120 20.0 N- (Trifluoroacetyl) - 22.79 1.8 ug/1 758689 ISTD04 24.99 8402690 20.0 3 -Isopropoxy-1,1,1,7 26.89 0.8 ug/1 327950 ISTD04 24.99 8402690 20.0 Benzoic acid, 2,5-bi 28.66 0.6 ug/1 235258 ISTD04 24.99 8402690 20.0 3 - Isopropoxv-1,1,1, 7 30.25 0.5 ug/1 204376 ISTD04 24.99 8402690 20.0 3 -Isopropoxy-1,1,1, 7 31.72 0.8 ug/1 161434 ISTD05 37.11 3951490 20.0 Chrysene -dl2 33.02 29.5 ug/1 5828990 ISTD05 37.11 3951490 20.0 3 - Isepropoxy- 1,1,1,7 34.38 0.5 ug/1 103268 ISTD05 37.11 3951490 20.0

30607.D GCMS0103.M Thu Jan 10 14:56:38 2002

NYC-WTC_000017191

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NYC-WTC_000017191Source: NYC Law Department, mirrored locally

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