GCMS method validation data, Jan 2002

NYC 9/11 Public Portal Document

DFTPP

Data File C:\HPCHEM\1\DATA\JAN0302\DFTPP.D Vial: 1 Acq On 3 Jan 2002 9:35 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundance TIC: DFTPP.D

1e+07 I | 8000000 /I i : eoooooo ‘ 4000000

i 2000000 . . „/ । 11 i i 11 „ , i . I'l'-rri । 4 i'i । j । 11 ■ — । 111 । । 11 rp 44 । । prr . 1 0- Time-> 24.20 24.40 24.60 24.80 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26.60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 Abundance Average of 26.047 to 26.120 min.: DFTPP.D ! 800000- 198

600000 69 127 442 400000 51 255

110 200000 275 224 93 167 i 0 ■ ■ । •+ 38 ■ kll L, I, 148, th 411/4.24, 148 ’Y180,. A 2111,242 _ 1, A,, 226310323338 352365 383,403.423 . -TTTTTgvffTTTrTTururuouumuutum1__UOSTTOSITTCs7Ttrnr1 ’ttr m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 26.047 to 26.120 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail

51 198 30 60 48.3 381035 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 59.5 469099 PASS 70 69 0.00 2 0.0 211 PASS 127 198 40 60 53.5 422351 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 788713 PASS 199 198 5 9 6.7 52678 PASS 275 198 10 30 20.3 160060 PASS 365 198 1 100 2.6 20380 PASS 441 443 0.01 100 94.8 72500 PASS 442 198 40 110 49.6 391054 PASS 443 442 17 23 19.6 76478 PASS

DFTPP.D GCMS0103.M Thu Jan 10 09:56:04 2002

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