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GCMS analysis report for sample AD30110, January 2002

Machine-extracted title · confidence 85%

Laboratory GCMS analysis report for sample AD30110 conducted on January 9, 2002, by analyst DLV.

NYC-WTC_000016891–000016907

Folder label: “GCMS X 12/12/01 A 12/20/01

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Scanned page image, NYC-WTC_000016906
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NYC 9/11 Public Portal Document . Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0302\30253.D Vial: 35 Acq On : 4 dan 2002 7:39 pm Operator: 209 GALOS Sample : goms scan 1/2a Inst. : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS OIE EIS SEO TO FOOT ISSESISEI SOE IO ISO ISS TOSI TORI IS III Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.17 0.47 ug/1 132034 + Naphthalene-de 15.12 Hit# of 5 ntative ID MW MolForm cas# Qual 1 Cyclopentagiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 N-(Triflugracetyl)-0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 47 3 N-(Triflforoacetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 47 4 3,4-Dihydroxybenzyl alcohol, tris(tr_ 356 C16H3203Si3 068595-79-9 46 Abundance ‘Scan 984 (14.170 min): 30253.D (-) m/z 73.00 100.00 5000: 267 | 355 48 54193 13180 14.00 1420. 1440.14.60 ie 228 ae m/z 267.00 37.26 mz> ___ 50100150200 __ 250 __300__350__400__450__500 ee #51266: Cyclopentasiloxane, decamethyl- | | 356 | 5000: | 267 | ? | |_13180_14.00 14.20 14.40 14.60 m/z 355.05 27.92 | pre BM, 323 bn 50. 100 150 200 250 300, 350, 400 450. 500. Abundance ‘W58807; N-{Trifluoracetyl) 0G" O*-tris(trimethyisilyljepin | ' B | | a8. 13.80 14.00 14.20 14.40 14.60) 000 m/z 74.00 10.06 ' ba 140104 281 480 I> 50100 150200250300 350400450500. ‘Abundance #58326: N-(Trifiuoroacetyl)-O,0'.0"-tris(trimethyislly|)no | 13.80 14.00 14.20 14.40 14.60 oo m/z 356.05 9.65) | ‘5000: | 7 | | 126147 193 265 eel S78. 481 | imiz—> 50 100 150. 200 250 300 350 400 450 500| 13.80 14.00 14.20 14.40 14.60) 30253.D GCMS1126.M Mon Jan 07 11:48:07 2002 Page 2 NYC-WTC_000016906

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NYC-WTC_000016906Source: NYC Law Department, mirrored locally

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