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GCMS analysis report for sample AD30117, January 2002

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Laboratory GCMS analysis report for sample AD30117 conducted on January 9, 2002, by analyst DLV.

NYC-WTC_000016773–000016782

Folder label: “GCMS X 12/12/01 A 12/19/01

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Scanned page image, NYC-WTC_000016781
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NYC 9/11 Public Portal Document | Library Search Compound Report . Data File : C:\HPCHEM\1\DATA\JAN0302\30117.D Vial: 10 Acq on : 3 dan 2002 7:21 pm Operator: 209 GALOS Sample : gems scan 12/12 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS ISIE IGCIITIO CIOS ISI II IGG OCIS ISIS TOTS IG IO IIIT TSE Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2 R.T. EstCone Area Relative to ISTD RT. 7.60 0.54 ug/l 196885 1,4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 2-Pentanone/“4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 40 2 Butane, 17thoxy- 102 C6H140 000628-81-9 9 3 3-Hydroy¥-2-pentanone 102 C5H1002 003142-66-3 9 _4 5-Hexex-2-one __ ___98 C6H100 . 000109-49-9 9 ‘Abundance, ‘Scan 278 (7.508 min}: S0T17.D ( m/z 49.05 100.003 | i 8 | | 5000: | 101 ho ] 7.20 7.40 7.60 7.80 8.00 (ie 38), St 72 ; lwen> 1020 30 4050 60 70. 60 180 110 | m/z 59.05 Susi2 ‘Abundance: ene ‘4-hydroxy-4-methyl- | | 5000. | j 59 7.20 740 TE 7.80_ 8. i z 100.9 20.464 i 2 ° 28 101 — 1020 30 408000 Abundancs GBC: Butane, ethos i 59 | . ot i 7.20 7.40 7.60 7.80 8.00 | 5000: m/z 58.0, 16.42% i | i | | aie "3 ar. 102 preerpreperepeereper ere pe ey fnz—> 10.20 30 40 50 60 70 80 % 100 110 bundanes #1691: SHydroxpZpentanone = i 7.20 740 7.60 _7.80__ 8.00 | m/z 56.00 7.96% | 5000. . 45 | 15 ii L 66 73 84 102 mer 10 20 30 40 50 60 70 80 "9030 o| 730740" 1.60_7.80 __ 8.00 30117.D GCMS0103.M Mon Jan 07 10:34:13 2002 Page 2 NYC-WTC_000016781

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NYC-WTC_000016781Source: NYC Law Department, mirrored locally

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