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GCMS analysis results for sample AD31278, Feb 25, 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31278 conducted on February 25, 2002.

NYC-WTC_000016407–000016422

Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\FEB1402\31278.D Vial: 26 Acq On : 15 Feb 2002 3:27 am Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 12.341 789 795 809 rBV 874210 2141292 73.94% 14.772% 2 15.986 1186 1192 1209 rBV 1362084 2695319 93.07% 18.595% 3 21.301 1765 1771 1791 rBV 1460570 2895974 100.00% 19.979% 4 25.753 2249 2256 2267 rBV2 1378088 2820999 97.41% 19.462% 5 30.830 2804 2809 2815 rVB 147460 279490 9.65% 1.928%

6 33.823 3128 3135 3155 rBV 995290 2143145 74.00% 14.785% 7 38.110 3593 3602 3621 rBV 512832 1519027 52.45% 10.479%

Sum of corrected areas: 14495246

31278.D GCMS0208.M Fri Feb 15 14:04:41 2002

NYC-WTC_000016420

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NYC-WTC_000016420Source: NYC Law Department, mirrored locally

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