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GCMS analysis summary, sample AD31377, Feb 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31377 showing surrogate recovery and unknown compounds from February 7, 2002.

NYC-WTC_000016136–000016148

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JANI502\31377.D Vial: 23 Acq On : 16 Jan 2002 8:28 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant. Time: Feb 4 14:44 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.84 178 452 N.D. 3 4) Anthracene 24.84 178 452 N.D. 35) Di-n-butylphthalate 26.80 149 4866 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 32.79 228 1910 N.D. 42) Bis(2-ethylhexyl)phthalate 33.11 149 3580 N.D. 43) Chrysene 32.79 228 1910 N.D. 45) Di-n-Octylphthalate 35.26 149 108 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 4 7) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 36.86 252 2043 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 31377.D GCMS1126.M Mon Feb 04 14:45:23 2002 Page 2

NYC-WTC_000016139

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NYC-WTC_000016139Source: NYC Law Department, mirrored locally

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