Laboratory report listing pesticide and organic compound concentrations in sample AD31339 analyzed on February 7, 2002.
NYC-WTC_000016087–000016095Folder label: “GCMS X 12/26/01 A 1/15-1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JANI502\31339.D Vial: 17 Acq On : 16 Jan 2002 2:37 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 4 14:29 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.50 152 764739 20.00 ug/1 -0.19 10) Naphthalene-d8 15.09 136 3015192 20.00 ug/1 -0.21 17) Acenaphthene-dl0 20.35 164 1544769 20.00 ug/1 -0.22 29) Phenanthrene-diO 24.77 188 2053840 20.00 ug/1 -0.22 38) Chrysene-dl2 32.80 240 1232434 20.00 ug/1 -0.23 44) Perylene-dl2 36.86 264 786122 20.00 ug/1 -0.26
System Monitoring Compounds 37) 2,4-DDD 29.86 235 107826 4.78 ug/mL -0.21 Spiked Amount 5.000 Recovery = 95.60%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.11 74 234 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.15 128 1504 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.73 165 290 N.D. 25) Diethylphthalate 21.90 149 423 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 31339.D GCMS1126.M Mon Feb 04 14:33:40 2002 Page 1
NYC-WTC_000016089
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NYC-WTC_000016169
GCMS analysis report for sample AD31376 showing surrogate recovery and unknown compounds from February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016251
GCMS analysis report for sample AD31365 showing surrogate recovery and unknown compounds from February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016204
Gas chromatography-mass spectrometry analysis of environmental sample AD31379 completed on 02/07/2002, showing 2,4-DDD surrogate recovery at 115%.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018353
Laboratory report documenting GCMS analysis of sample AD31457 conducted on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016575
Laboratory report for DEP sample AD31464 identifying unknown compounds and surrogate recovery results from February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018396
Laboratory report documenting GCMS analysis of sample AD31467 conducted on February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016213
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31380 conducted on February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016195
GCMS analysis report for sample AD31378 showing surrogate recovery and unknown compounds from February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016223
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AD31348 conducted on February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016178
GCMS analysis report for sample AD31349 showing surrogate recovery and unknown compounds from February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016584
Laboratory report for DEP sample AD31433 identifying unknown compounds and surrogate recovery results from February 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036371
Laboratory GCMS analysis report for sample AD29290 conducted on January 4, 2002, showing unknown compounds.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000016055
DEP GCMS analysis log covering samples processed between late December 2001 and mid-January 2002.
Filed in the same folder
NYC-WTC_000016056
Technical log detailing extraction rates, volumes, and pH settings used during sample preparation for GCMS analysis.
Filed in the same folder
NYC-WTC_000016058
Documentation of instrument settings and calibration parameters for Method 508 analysis conducted in early 2002.
Filed in the same folder
NYC-WTC_000016061
Calibration data sheet listing response factors for various organic compounds including nitrosamines and chlorinated benzenes.
Filed in the same folder
NYC-WTC_000016065
Calibration report showing retention times and response factors for deuterated internal standards used in PAH analysis.
Filed in the same folder