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GCMS reference standard results for organic compounds, February 2002

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Reference analysis report confirming instrument performance with measured values for nitrosamines and chlorinated solvents.

NYC-WTC_000016068–000016072

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JAN1502\REFB.D Vial: 7 Acq On : 15 Jan 2002 4:48 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 412:512002 (Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.40 168 110888 2.97 ug/1 98 31) 4-Bromophenyl-phenylether 23.46 248 85792 4.15 ug/1 99 32) Hexachlorobenzene 23.88 284 101024 4.45 ug/1 97 33) Phenanthrene 24.84 178 476361 4.28 ug/1 99 34) Anthracene 24.97 178 426169 3.84 ug/1 99 35) Di -n-butylphthalate 26.79 149 692753 4.68 ug/1 99 36) Fluoranthene 28.45 202 446391 4.16 ug/1 97 39) Pyrene 29.11 202 465537 4.22 ug/1 98 40) Butylbenzylphthalate 31.30 149 236061 4.10 ug/1 99 41) Benzo(a)anthracene 32.75 228 302901 3.98 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.10 14 9 347527 4.47 ug/1 99 43) Chrysene 32.87 228 321285 4.31 ug/1 99 45) Di -n-Octylphthalate 34.85 149 383006 3.31 ug/1 # 95 46) Benzo(b)fluoranthene 35.83 252 262789 4.01 ug/1 97 47) Benzo(k)fluoranthene 35.89 252 315870 4.70 ug/1 96 48) Benzo(a)pyrene 36.70 252 184397 3.24 ug/1 98 49) Indeno(1,2,3-cd)pyrene 40.42 276 214133 3.76 ug/1 94 50) Dibenz(a,h)anthracene 40.48 278 177766 3.99 ug/1 99 51) Benzo(g,h,i)perylene 41.46 276 198940 4.09 ug/1 97

(#) = qualifier out of range (m) = manual integration REFB.D GCMS1126.M Mon Feb 04 12:53:53 2002 Page 2

NYC-WTC_000016071

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NYC-WTC_000016071Source: NYC Law Department, mirrored locally

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