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← Document results/DEP Box 16/GCMS X 12/26/01 A 1/15-1/16/02
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GCMS instrument extraction parameters and settings

Machine-extracted title · confidence 90%

Technical log detailing extraction rates, volumes, and pH settings used during sample preparation for GCMS analysis.

NYC-WTC_000016056–000016057

Folder label: “GCMS X 12/26/01 A 1/15-1/16/02

Page image
Scanned page image, NYC-WTC_000016057
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

DFTPP

Data File C: \HPCHEM\1\DATA\DEC1801\DFTPP1 .D Vial: 1 Acq On 19 Dec 2001 8:42 am Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table

Abundange TIC: DFTPP1.D

8000000

6000000

4000000

2000000

Tlme-> .... .A................. ......._A.......... 0+ 24.40 24.60 24.80 25.00 25.20 25.40 25.60 25.80 26.00 26.20 26.40 26*60 26.80 27.00 27.20 27.40 27.60 27.80 28.00 Abundance Average of 26.216 to 26.262 min.: DFTPP1.D 198 800000

600000 442 69 127 255 400000 51 110 200000 275 224 93 .. 38 0 • *'11 • • H h-p hert" , 148 1671 80141.248.4 „-H---++*========21$219822229,352365,383,403.423.4 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 26.216 to 26.262 min.

Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit % Limit% Abn% Abn Pass/Fail

51 198 30 60 36.9 325045 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 46.2 406955 PASS 70 69 0.00 2 0.0 56 PASS 127 198 40 60 48.4 426496 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 881184 PASS 199 198 5 9 6.6 58321 PASS 275 198 10 30 21.1 185931 PASS 365 198 1 100 2.5 21764 PASS 441 443 0.01 100 92.7 86832 PASS 442 198 40 110 54.7 481835 PASS 443 442 17 23 19.4 93632 PASS

DFTPP1.D GCMS1126.M Thu Jan 03 10:06:05 2002

NYC-WTC_0000 16057

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NYC-WTC_000016057Source: NYC Law Department, mirrored locally

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