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Pesticide analysis results, sample AE11755, May 2002

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Laboratory report listing pesticide and organic compound concentrations in sample AE11755 analyzed between May 10 and May 13, 2002.

NYC-WTC_000015992–000016005

Folder label: “525 X 5/10/02 A 5/13/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\051302\LBB0513.D Vial: 12 ' Acq On : 13 May 2002 8:50 pm Operator: Bohlk / Inst 213 Sample : LB 5/13/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 13.126 221 226 232 rVB 1352058 2341820 54.68% 8.864% 2 18.214 781 787 793 rBV 2246670 3994780 93.27% 15.121% 3 18.550 819 824 829 rVB 402132 638946 14.92% 2.419% 4 19.983 979 982 986 rBV 43730 64380 1.50% 0.244% 5 22.532 1257 1263 1274 rBV2 2156101 4283093 100.00% 16.212%

6 22.749 1284 1287 1291 rVB2 29213 43678 1.02% 0.165% 7 26.650 1711 1717 1730 rBV 2125483 3965865 92.59% 15.012% 8 27.420 1797 1802 1812 rBV 1946880 3762984 87.86% 14.244% 9 29.597 2037 2042 2057 rBV 1117819 2229614 52.06% 8.440% 10 30.323 2115 2122 2140 rBV2 1349582 3198939 74.69% 12.109%

11 30.976 2189 2194 2201 rBV2 20351 49282 1.15% 0.187% 12 34.332 2558 2564 2580 rBV2 618332 1845128 43.08% 6.984%

Sum of corrected areas: 26418509

5BB0513.D 050802.M Tue May 14 11:03:02 2002 Page 1

NYC-WTC_000015994

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NYC-WTC_000015994Source: NYC Law Department, mirrored locally

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GCMS blank results, April 2002 · Box DEP Box 57

NYC-WTC_000060990

Gas chromatography mass spectrometry blank analysis report showing non-detect levels for various organic compounds.

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