GCMS quantitation report, May 22 2002

NYC 9/11 Public Portal Document LbU area Percent KepOrt Data File : C:\MSDCHEM\l\DATA\052202\11905.D Vial: 12 Acq On : 22 May 2002 10:47 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.708 91 107 109 PV 4 23962 795749 1.69% 0.290% 2 3.726 109 110 112 W 2 25149 259429 0.55% 0.095% 3 3.761 112 116 126 W 7 24864 1106454 2.35% 0.404% 4 3.843 126 130 137 W 5 21523 790006 1.68% 0.288% 5 3.890 137 138 151 W 9 19786 926280 1.97% 0.338%

6 3.978 151 153 160 W 4 17095 480104 1.02% 0.175% 7 4.290 200 206 214 W 2 23653 683855 1.45% 0.249% 8 4.531 243 247 253 W 7 6981 205309 0.44% 0.075% 9 4.907 307 311 319 W 7 3348 42102 0.09% 0.015% 10 5.377 371 391 406 BV 5 5118 171956 0.37% 0.063%

11 5.941 481 487 507 PV 498062 9402191 20.00% 3.429% 12 6.064 507 508 512 W 4 2803 35926 0.08% 0.013% 13 7.703 781 787 799 PV 4 6434 167631 0.36% 0.061% 14 9.901 1148 1161 1176 PV 1624467 30967774 65.86% 11.294% 15 12.374 1575 1582 1590 PV 126397 1933477 4.11% 0.705%

16 13.397 1742 1756 1777 PV 2246529 41733323 88.76% 15.220% 17 13.550 1777 1782 1788 W 6517 98362 0.21% 0.036% 18 15.659 2124 2141 2147 PV 6 1978 40754 0.09% 0.015% 19 16.705 2309 2319 2328 PV 4 3710 69297 0.15% 0.025% 20 17.110 2383 2388 2395 W 3 6397 104846 0.22% 0.038%

21 17.621 2469 2475 2481 PV 2 3454 57197 0.12% 0.021% 22 18.532 2620 2630 2653 W 2455876 46349212 98.57% 16.903% 23 18.779 2661 2672 2679 PV 4 3254 57174 0.12% 0.021% 24 20.101 2882 2897 2911 BV 520832 8532071 18.15% 3.112% 25 20.283 2925 2928 2947 VB 4 2984 50679 0.11% 0.018%

26 20.506 2950 2966 2979 BV 1261142 24001739 51.05% 8.753% 27 21.358 3103 3111 3117 PV 2 10907 182239 0.39% 0.066% 28 21.722 3161 3173 3178 W 4 3547 69654 0.15% 0.025% 29 22.539 3305 3312 3322 W 2 19308 346348 0.74% 0.126% 30 22.915 3365 3376 3396 PV 2 2250226 47020310 100.00% 17.148%

31 23.068 3396 3402 3412 W 4 16617 335992 0.71% 0.123% 32 29.942 4566 4572 4578 W 3 2148 48143 0.10% 0.018% 33 30.765 4692 4712 4760 PV 2 1568737 34611115 73.61% 12.623% 34 31.335 4801 4809 4816 PV 5 2440 47344 0.10% 0.017% 35 34.660 5360 5375 5410 W 2 993394 22300862 47.43% 8.133%

36 34.872 5410 5411 5420 W 7 3140 74941 0.16% 0.027% 37 35.377 5482 5497 5503 W 8 2017 71159 0.15% 0.026%

11905.D 052202.M Tue May 28 12:11:51 2002 Page 1

NYC-WTC_000015609