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GCMS sample AE11905 results, June 6 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis report for sample AE11905 detecting unknown compounds and surrogates on June 6, 2002.

NYC-WTC_000015581–000015605

Folder label: “GCMS X 6/4/02 A 6/4/02

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Scanned page image, NYC-WTC_000015586
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C: \MSDCHEM\1\DATA\060402\11905.D Vial: 8 Acq On 4 Jun 2002 9:33 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corf. corr. % of # min scan scan scan TY height area % max. total

1 3.385 50 52 58 PV 3 2355 33953 0.08% 0.016% 2 3.479 63 68 77 W 7 7656 187588 0.47% 0.087% 3 3.725 89 110 111 PV 3 29100 1177755 2.92% 0.546% 4 3.743 111 113 114 W 2 28360 305005 0.76% 0.141% 5 3.761 114 116 130 W 8 28366 1475277 3.66% 0.684%

6 3.855 130 132 137 W 3 26219 602284 1.49% 0.279% 7 3.896 137 139 144 W 5 23769 545493 1.35% 0.253% 8 3.931 144 145 148 W 3 22796 291377 0.72% 0.135% 9 3.960 148 150 153 W 3 22708 405265 1.01% 0.188% 10 3.984 153 154 165 W 5 21869 828142 2.05% 0.384%

11 4.178 184 187 196 W 6 17072 650121 1.61% 0.301% 12 4.254 196 200 202 W 4 15066 321302 0.80% 0.149% 13 4.278 202 204 207 W 3 15502 233642 0.58% 0.108% 14 4.524 242 246 251 W 6 14078 397501 0.99% 0.184% 15 5.218 362 364 365 W 2 3758 31911 0.08% 0.015%

16 5.341 381 385 393 W 5 3492 90316 0.22% 0.042% 17 5.952 483 489 499 PV 14329 360914 0.90% 0.167% 18 6.023 499 501 505 W 5 ' 3101 39678 0.10% 0.018% 19 8.702 945 957 968 PV 4 4436 133063 0.33% 0.062% 20 9.895 1148 1160 1183 PV 1356736 27231986 67.57% 12.619%

21 12.368 1573 1581 1588 PV 5987 89640 0.22% 0.042% 22 13.391 1742 1755 1771 BV 1999545 36494234 90.55% 16.910% 23 13.544 1774 1781 1786 W 2 5083 87548 0.22% 0.041% 24 15.659 2136 2141 2145 PV 2 1623 25358 0.06% 0.012% 25 16.705 2314 2319 2326 W 2 3014 47583 0.12% 0.022%

26 17.104 2380 2387 2396 W 3 5961 100897 0.25% 0.047% 27 17.621 2469 2475 2480 W 5 3217 54871 0.14% 0.025% 28 18.526 2611 2629 2644 PV 2121899 40263184 99.91% 18.657% 29 20.101 2889 2897 2901 PV 4 1803 26441 0.07% 0.012% 30 20.500 2951 2965 2979 PV 1113037 20816955 51.65% 9.646%

31 21.352 3103 3110 3127 PV 3 9212 147028 0.36% 0.068% 32 22.533 3301 3311 3321 PV 3 13943 252163 0.63% 0.117% 33 22.903 3361 3374 3393 PV 2 1962260 40301209 100.00% 18.674% 34 23.062 3393 3401 3408 W 14589 309572 0.77% 0.143% 35 25.042 3733 3738 3748 W 3 2659 55192 0.14% 0.026%

36 30.753 4696 4710 4741 PV 2 1163276 25930620 64.34% 12.016% 37 30.947 4741 4743 4753 W 6 2364 47523 0.12% 0.022%

11905.D 060302.M Wed Jun 05 14:03:34 2002 Page 1

NYC-WTC_000015586

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NYC-WTC_000015586Source: NYC Law Department, mirrored locally

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