GCMS sample AE12743 results, June 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\060602\12761.D Vial: 7 Acq On 6 Jun 2002 4:11 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan '5 Library : C: \DATABASE\NI ST9 8 . L ********************************************************************* Peak Number 2 Methylene Chloride Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T.

3.53 0.27 ug/L 181201 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methylene Chloride 84 CH2C12 000075-09-2 50 2 Methylene Chloride 84 CH2C12 000075-09-2 7 3 DL-Norleucine 131 C6H13NO2 000616-06-8 4 4 Methylene Chloride 84 CH2C12 000075-09-2 4 Abundance Scan 77 (3.532 min): 12761 .D (-75) (-) m/z 86.00 00.00% 49 85

5000

74 42 3 20 3.40 3.60 3.80 ' '

m/z-> 01 4 10 20 30 40 59 | TTP ‘l2-r11r2t1-1111111111313T 50 60 70 80 90 100 110 120 130 m/z 49.10 . 93.98% Abundance #111040: Methylene Chloride 49 84

5000- 320 3.40 3.60 3.80 35 m/z 84.00 90.97%

miz-> 01 — 14 28 10 20 30 40 1414450 60 7070 80 #mmm ' ■ i ■ ■ ■' I ‘ ■ ■ ■ i ■ 90 100 110 120 130 Abundance #12327: Methylene Chloride 49 84 3.20 ' 3.40 3.60 ' 3.80 ‘ ' 5000 m/z 55.10 25.50%

Of 14 24 35 41 I,............ 70........ . I I | l‘l 1 1 | 1 t IT| J |’ 1 1 ’ll [ Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #34635: DL-Norleucine 1 i 1 1 ■ ‘ i ' ■ 86 3.20 3.40 3.60 3.80 m/ z 74.00 21.92% 30 5000

74

0 np r i1 10 18

20 4—56,..67,4 11—f 99 113 T10B—-10331--n———m—p33 132 1—T ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 3.20 3.40 3.60 3.80

12761.D 060302.M Mon Jun 10 10:25:02 2002 Page 5

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