GCMS reference standard results, June 10 2002

NYC 9/11 Public Portal Document LSC Area Percent Keport

Data File C:\MSDCHEM\1\DATA\060602\12743.D Vial: 6 Acq On 6 Jun 2002 3:22 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.473 64 67 82 PV 6 8341 219380 0.51% 0.092% 2 3.725 93 110 116 PV 6 70065 3957624 9.15% 1.658% 3 3.772 116 118 121 W 4 67560 1188493 2.75% 0.498% 4 3.796 121 122 125 W 3 65095 895788 2.07% 0.375% 5 3.825 125 127 130 W 4 63136 1118306 2.59% 0.469%

6 3.855 130 132 134 W 3 59870 802416 1.85% 0.336% 7 3.878 134 136 148 W 6 58814 2652793 6.13% 1.111% 8 3.966 148 151 153 W 3 54723 1082893 2.50% 0.454% 9 3.990 153 155 159 W 3 52146 970159 2.24% 0.406% 10 4.107 171 175 187 W 8 48599 2394196 5.53% 1.003%

11 4.354 215 217 223 W 5 32723 818959 1.89% 0.343% 12 4.519 243 245 255 W 5 31433 1250871 2.89% 0.524% 13 4.589 255 257 268 W 5 24795 1034260 2.39% 0.433% 14 4.666 268 270 272 W 23132 307983 0.71% 0.129% 15 4.953 316 319 322 W 4 13222 233689 0.54% 0.098%

16 4.983 322 324 329 W 4 12871 288224 0.67% 0.121% 17 5.183 356 358 361 W 4 8754 122419 0.28% 0.051% 18 5.341 382 385 386 W 2 7555 95840 0.22% 0.040% 19 5.371 386 390 401 W 2 7333 294141 0.68% 0.123% 20 5.559 420 422 433 W 9 4140 150344 0.35% 0.063%

21 5.782 458 460 462 W 3 2758 25027 0.06% 0.010% 22 5.982 489 494 506 PV 5 4697 154898 0.36% 0.065% 23 7.832 804 809 819 W 8 2772 70788 0.16% 0.030% 24 9.213 1036 1044 1061 PV 2 11945 214060 0.49% 0.090% 25 9.895 1148 1160 1179 PV 1392350 28546058 65.99% 11.959%

26 10.165 1201 1206 1215 W 5 4326 100644 0.23% 0.042% 27 12.368 1575 1581 1590 W 11987 188651 0.44% 0.079% 28 13.162 1711 1716 1721 PV 3 3315 60562 0.14% 0.025% 29 13.391 1745 1755 1776 W 2107805 38548833 89.11% 16.150% 30 13.544 1776 1781 1789 W 2 5985 120827 0.28% 0.051%

31 14.008 1844 1860 1870 W 4 7642 150841 0.35% 0.063% 32 15.441 2098 2104 2111 W 13488 209178 0.48% 0.088% 33 15.659 2130 2141 2151 W 6 1684 37614 0.09% 0.016% 34 16.305 2245 2251 2263 W 2 13342 297760 0.69% 0.125% 35 16.699 2311 2318 2331 PV 3 3357 76754 0.18% 0.032%

36 17.104 2383 2387 2395 PV 2 5990 88878 0.21% 0.037% 37 17.621 2470 2475 2485 W 6 2478 46046 0.11% 0.019%

12743.D 060302.M Mon Jun 10 10:21:37 2002 Page 1

NYC-WTC_000015386