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GCMS analysis results for unknown compounds, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE12738 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015282–000015310

Folder label: “GCMS X 6/3/02 A 6/7/02

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Scanned page image, NYC-WTC_000015287
OCR text

OCR status: junk · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\060702\12739.D Vial: 15 Acq On 7 Jun 2002 7:58 pm Operator: Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.214 21 23 30 PV 3 2577 23824 0.05% 0.009% 2 3.479 63 68 78 PV 4 13104 303009 0.63% 0.109% 3 3.549 78 80 83 W 3 4448 43207 0.09% 0.015% 4 3.726 92 110 124 PV 4 74081 6125896 12.66% 2.196% 5 3.814 124 125 145 W 5 69970 4786588 9.89% 1.716%

6 3.943 145 147 151 W 4 59941 1318605 2.73% 0.473% 7 3.984 151 154 159 W 6 57879 1548926 3.20% 0.555% 8 4.025 159 161 166 W 4 55047 1235676 2.55% 0.443% 9 4.061 166 167 174 W 5 52185 1414999 2.92% 0.507% 10 4.119 174 177 186 W 7 53645 2134915 4.41% 0.765%

11 4.249 198 199 206 W 4 43677 1169712 2.42% 0.419% 12 4.525 244 246 261 W 8 34868 1783895 3.69% 0.639% 13 4.713 276 278 282 W 4 22372 426647 0.88% 0.153% 14 5.106 343 345 353 W 4 13383 361505 0.75% 0.130% 15 5.876 474 476 478 W 2 2962 21394 0.04% 0.008%

16 5.911 478 482 484 PV 5 2495 33430 0.07% 0.012% 17 5.947 484 488 513 W 21767 640676 1.32% 0.230% 18 6.769 626 628 632 PV 5 2324 27100 0.06% 0.010% 19 6.804 632 634 640 W 6 2758 44608 0.09% 0.016% 20 6.863 640 644 649 W 6 2439 34350 0.07% 0.012%

21 8.702 951 957 970 PV 2 11497 262446 0.54% 0.094% 22 8.990 1002 1006 1013 W 6 2707 75250 0.16% 0.027% 23 9.213 1037 1044 1055 W 4 7414 151692 0.31% 0.054% 24 9.895 1146 1160 1178 PV 1617082 31870204 65.87% 11.423% 25 10.007 1178 1179 1189 W 6 2807 70797 0.15% 0.025%

26 10.089 1189 1193 1201 W 8 2568 57351 0.12% 0.021% 27 11.828 1484 1489 1498 PV 7 2195 41744 0.09% 0.015% 28 12.369 1573 1581 1586 PV 2 23261 354766 0.73% 0.127% 29 13.391 1738 1755 1776 PV 2330894 42997222 88.86% 15.411% 30 13.544 1776 1781 1787 W 3 6511 110461 0.23% 0.040%

31 14.002 1855 1859 1868 W 3 2384 39818 0.08% 0.014% 32 15.441 2098 2104 2121 W 12145 202286 0.42% 0.073% 33 15.653 2136 2140 2145 PV 7 2088 39825 0.08% 0.014% 34 16.699 2314 2318 2324 PV 3 3665 58196 0.12% 0.021% 35 17.104 2376 2387 2395 PV 4 8491 145375 0.30% 0.052%

36 17.615 2465 2474 2483 PV 4 4471 77284 0.16% 0.028% 37 18.191 2559 2572 2577 W 3 4194 77483 0.16% 0.028%

12739.D 060302.M Mon Jun 10 11:50:59 2002 Page 1

NYC-WTC_000015287

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NYC-WTC_000015287Source: NYC Law Department, mirrored locally

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