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GCMS analysis results for unknown compounds, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE12736 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015224–000015252

Folder label: “GCMS X 6/3/02 A 6/7/02

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Scanned page image, NYC-WTC_000015229
OCR text

OCR status: junk · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\1\DATA\060702\12737.D Vial: 13 Acq On 7 Jun 2002 6:21 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.467 64 66 74 PV 5 5463 122909 0.36% 0.066% 2 3.726 93 110 123 PV 4 60840 4700802 13.88% 2.516% 3 3.808 123 124 134 W 3 55457 2114249 6.24% 1.132% 4 3.878 134 136 140 W 5 50800 978613 2.89% 0.524% 5 3.908 140 141 147 W 4 48723 1249100 3.69% 0.669%

6 3.955 147 149 161 W 5 47455 2212326 6.53% 1.184% 7 4.031 161 162 172 W 6 43147 1517163 4.48% 0.812% 8 4.102 172 174 186 W 6 41302 1956887 5.78% 1.047% 9 4.343 213 215 217 W 3 29880 424169 1.25% 0.227% 10 4.513 242 244 251 W 3 26473 840596 2.48% 0.450%

11 4.848 299 301 306 W 6 15104 333471 0.98% 0.178% 12 5.952 484 489 502 W 3 10439 353498 1.04% 0.189% 13 6.240 536 538 547 PV 6 2022 48947 0.14% 0.026% 14 6.910 650 652 653 PV 2 1740 8656 0.03% 0.005% 15 8.702 945 957 966 PV 3 5584 147262 0.43% 0.079%

16 9.020 1000 1011 1013 W 8 2050 55411 0.16% 0.030% 17 9.213 1034 1044 1056 PV 14525 270555 0.80% 0.145% 18 9.895 1150 1160 1176 PV 1065681 22142505 65.40% 11.850% 19 12.369 1574 1581 1587 W 46015 724253 2.14% 0.388% 20 13.385 1743 1754 1772 W 1671637 30102877 88.91% 16.111%

21 13.544 1776 1781 1786 W 4273 85855 0.25% 0.046% 22 14.002 1849 1859 1866 W 5 3479 66752 0.20% 0.036% 23 15.442 2092 2104 2116 PV 45158 675796 2.00% 0.362% 24 16.699 2312 2318 2324 PV 2 2266 39663 0.12% 0.021% 25 17.104 2378 2387 2392 W 5 3849 67257 0.20% 0.036%

26 17.621 2467 2475 2482 PV 6 1989 38861 0.11% 0.021% 27 18.191 2566 2572 2582 W 15646 244645 0.72% 0.131% 28 18.520 2619 2628 2645 PV 1819296 33857020 100.00% 18.120% 29 19.143 2727 2734 2749 PV 2 11319 216442 0.64% 0.116% 30 20.500 2943 2965 2982 PV 867699 16265744 48.04% 8.705%

31 20.636 2982 2988 2995 PV 6635 97367 0.29% 0.052% 32 21.352 3102 3110 3116 BV 4 5148 82256 0.24% 0.044% 33 22.533 3303 3311 3321 BV 2 10282 202136 0.60% 0.108% 34 22.751 3340 3348 3355 W 3 2329 43328 0.13% 0.023% 35 22.904 3362 3374 3395 W 2 1676392 33756358 99.70% 18.066%

36 23.062 3395 3401 3418 W 12179 272432 0.80% 0.146% 37 30.753 4699 4710 4759 PV 2 859993 19662572 58.08% 10.523%

12737.D 060302.M Mon Jun 10 11:23:46 2002 Page 1

NYC-WTC_000015229

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NYC-WTC_000015229Source: NYC Law Department, mirrored locally

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