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GCMS analysis results for unknown compounds, June 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE12736 with surrogate recovery data and identification of unknown compounds.

NYC-WTC_000015224–000015252

Folder label: “GCMS X 6/3/02 A 6/7/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\060702\12737.D Vial: 13 Acq On 7 Jun 2002 6:21 pm Operator: Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Jun 10 11:18:59 2002 Quant Results File: 060302.RES Quant Method : C:\MSDCHEM\l\METHQDS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu Jun 06 15:03:45 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-dichlorobenzene-d4 9.89 152 3757523 40.00 ug/L 0.00 10) Napthalene-d8 13.39 136 14960005 40.00 ug/L 0.00 17) Acenapthalene-dlO 18.52 164 8290854 40.00 ug/L 0.00 29) Phenanthranene-dlO 22.90 188 12524623 40.00 ug/L 0.00 37) Chrysene-dl2 30.75 240 6353980 40.00 ug/L 0.00 43) Perylene-dl2 34.65 264 2978112 40.00 ug/L 0.00 System Monitoring Compounds 27) TCMX 20.50 209 1654871 27.82 ug/L 0.00 Spiked Amount 40.000 Recovery 69.55% Target Compounds Qvalue 2) n-nitros-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 . 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'oxybis(1-Chloropropane 0.00 45 0 N.D. 8) N-nitroso-di-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Napthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) 2-Chloronaphthalene 0.00 162 0 N.D. 19) Dimethylphthalate 0.00 163 0 N.D. 20) 2,6-Dinitrotoluene 0.00 165 0 N.D. 21) Acenapthylene 0.00 152 0 N.D. 22) Acenapthalene 0.00 153 0 N.D. 23) 2,4-Dinitrotoluene 0.00 165 0 N.D. 24) Diethylphthalate 0.00 149 0 N.D. 25) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 26) Fluorene 0.00 166 0 N.D. 28) Azobenzene 20.50 77 25867 N.D. 30) Nnitrosodiphenylamine 20.50 169 28727 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 0.00 149 0 N.D. (#) = qualifier out of range (m) = manual integration 12737.D 060302.M Mon Jun 10 11:19:33 2002 Page 1

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NYC-WTC_000015226Source: NYC Law Department, mirrored locally

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