GCMS reference analysis results for volatile organics, June 2002

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Data File C:\MSDCHEM\1\DATA\060702\12735.D Vial: 11 Acq On 7 Jun 2002 4:43 pm Operator: Sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.479 64 68 79 PV 4 7079 160920 0.37% 0.065% 2 3.725 93 110 122 PV 4 65742 5012599 11.65% 2.032% 3 3.802 122 123 127 W 4 61963 1041944 2.42% 0.422% 4 3.843 127 130 146 W 8 59045 3734365 8.68% 1.514% 5 3.955 146 149 158 W 5 52758 2044712 4.75% 0.829%

6 4.013 158 159 167 W 3 50025 1492190 3.47% 0.605% 7 4.072 167 169 173 W 4 43659 893739 2.08% 0.362% 8 4.107 173 175 180 W 6 44086 980924 2.28% 0.398% 9 4.143 180 181 184 W 3 41560 694183 1.61% 0.281% 10 4.225 193 195 197 W 2 37332 553843 1.29% 0.225%

11 4.254 197 200 208 W 5 35798 1294849 3.01% 0.525% 12 4.513 240 244 249 W 6 27995 795160 1.85% 0.322% 13 4.648 265 267 278 W 5 21486 838582 1.95% 0.340% 14 5.136 348 350 355 W 2 9721 190181 0.44% 0.077% 15 5.183 355 358 360 W 3 7741 115421 0.27% 0.047%

16 5.206 360 362 368 W 4 7702 201859 0.47% 0.082% 17 5.365 385 389 402 W 8 6980 333712 0.78% 0.135% 18 5.459 402 405 410 W 3 4878 106151 0.25% 0.043% 19 5.723 446 450 461 W 8 3241 108054 0.25% 0.044% 20 5.829 466 468 474 PV 5 1824 30318 0.07% 0.012%

21 5.952 483 489 494 W 2 15157 304895 0.71% 0.124% 22 5.987 494 495 500 W 2 8580 102411 0.24% 0.042% 23 6.134 518 520 526 PV 6 1736 16177 0.04% 0.007% 24 6.792 627 632 645 PV 9 2001 44270 0.10% 0.018% 25 7.233 700 707 714 W 7 3437 70434 0.16% 0.029%

26 7.621 772 773 777 PV 3 1706 17523 0.04% 0.007% 27 7.938 824 827 829 W 4 2053 17930 0.04% 0.007% 28 8.702 951 957 967 PV 3 7708 183347 0.43% 0.074% 29 9.219 1034 1045 1058 PV 10253 214125 0.50% 0.087% 30 9.895 1151 1160 1178 PV 1387204 27918919 64.87% 11.318%

31 11.828 1482 1489 1495 W 5 3131 50970 0.12% 0.021% 32 12.368 1575 1581 1587 PV 2 12666 196352 0.46% 0.080% 33 13.391 1728 1755 1772 PV 2043984 37909654 88.08% 15.368% 34 13.544 1776 1781 1791 W 6739 133008 0.31% 0.054% 35 14.002 1852 1859 1873 PV 5 2415 49217 0.11% 0.020%

36 15.659 2127 2141 2145 PV 5 1838 37498 0.09% 0.015% 37 16.705 2312 2319 2328 W 4 3179 64877 0.15% 0.026%

12735.D 060302.M Mon Jun 10 11:22:42 2002 Page 1

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