GCMS blank analysis report for sample AE12735, June 2002

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Data File C:\MSDCHEM\1\DATA\0 6 0 7 0 2\LBA.D Vial: 10 Acq On 7 Jun 2002 3:55 pm Operator: Sample gc/ms scan 6/3 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.220 22 24 39 PV 3 2725 65715 0.16% 0.027% 2 3.473 64 67 72 PV 5 6918 117033 0.28% 0.049% 3 3.708 94 107 110 PV 4 62978 2167803 5.18% 0.905% 4 3.737 110 112 116 W 3 63695 1414125 3.38% 0.591% 5 3.772 116 118 121 W 4 61526 1012337 2.42% 0.423%

6 3.802 121 123 147 W 7 60993 5028360 12.01% 2.100% 7 3.949 147 148 160 W 5 50782 2151734 5.14% 0.899% 8 4.025 160 161 166 W 4 45790 989169 2.36% 0.413% 9 4.084 170 171 174 W 2 42843 679824 1.62% 0.284% 10 4.125 174 178 188 W 5 41536 1805290 4.31% 0.754%

11 4.525 242 246 259 W 8 26516 1407306 3.36% 0.588% 12 5.018 329 330 333 W 3 10252 133919 0.32% 0.056% 13 5.189 357 359 361 W 3 7189 84931 0.20% 0.035% 14 5.353 385 387 397 W 6 6902 219325 0.52% 0.092% 15 5.482 406 409 412 W 4 3998 60860 0.15% 0.025%

16 5.952 482 489 513 W 3 12030 419264 1.00% 0.175% 17 6.411 563 567 569 PV 5 1883 25660 0.06% 0.011% 18 8.702 951 957 969 PV 2 7913 191427 0.46% 0.080% 19 9.008 999 1009 1016 PV 7 2268 75255 0.18% 0.031% 20 9.213 1037 1044 1054 W 3 8234 163301 0.39% 0.068%

21 9.895 1149 1160 1185 PV 1374611 27763179 66.33% 11.596% 22 11.828 1485 1489 1504 PB 7 2003 38959 0.09% 0.016% 23 12.368 1574 1581 1593 PV 7798 125189 0.30% 0.052% 24 13.391 1745 1755 1774 PV 2058254 37438429 89.44% 15.637% 25 13.538 1774 1780 1788 W 5659 112023 0.27% 0.047%

26 15.653 2132 2140 2144 W 2 1727 24875 0.06% 0.010% 27 16.699 2310 2318 2324 W 4 3121 51205 0.12% 0.021% 28 17.104 2378 2387 2392 W 3 4466 81592 0.19% 0.034% 29 17.615 2466 2474 2479 W 5 2414 39815 0.10% 0.017% 30 18.526 2614 2629 2650 BV 2175663 41692729 99.60% 17.413%

31 19.143 2711 2734 2739 W 4 1809 39038 0.09%, 0.016% 32 20.500 2951 2965 2978 W 1018639 19308275 46.13% 8.064% 33 21.352 3104 3110 3120 W 4 7189 116768 0.28% 0.049% 34 21.711 3165 3171 3175 PV 4 2245 34856 0.08% 0.015% 35 22.533 3300 3311 3319 PV 2 14577 264227 0.63% 0.110%

36 22.909 3363 3375 3395 PV 2 2019596 41858972 100.00% 17.483% 37 23.062 3395 3401 3415 W 16284 328576 0.78% 0.137%

LBA.D 060302.M Mon Jun 10 11:27:06 2002 Page 1

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