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GCMS blank analysis report for sample AE12224, June 2002

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Laboratory report documenting a method blank analysis for GCMS testing of sample AE12224 to verify absence of contamination on June 3, 2002.

NYC-WTC_000015040–000015053

Folder label: “GCMS X 5/31/02 A 6/3/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\JUN0302\LB.D Vial: 3 Acq On 3 Jun 2002 10:40 am Operator: Morgan Sample gc/ms scan 5/31 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.067 326 329 338 rBV 20338 55815 1.43% 0.248% 2 12.070 759 765 785 rBV 1121231 2736000 69.90% 12.142% 3 15.696 1154 1160 1178 rBV 1777834 3762604 96.13% 16.698% 4 20.993 1730 1737 1758 rBV 1840002 3884341 99.24% 17.239% 5 23.132 1962 1970 1979 rBV 969364 2027335 51.80% 8.997% 6 25.427 2213 2220 2232 rBV2 1831910 3914061 100.00% 17.371% 7 33.478 3090 3097 3111 rBV2 1294222 2962603 75.69% 13.148% 8 35.948 3361 3366 3380 rBV2 27813 98627 2.52% 0.438% 9 37.150 3490 3497 3512 rBV2 38945 174816 4.47% 0.776% 10 37.655 3544 3552 3565 rBV2 762755 2231750 57.02% 9.904% 11 38.555 3642 3650 3662 rBV2 37252 184218 4.71% 0.818% 12 40.244 3826 3834 3853 rBV2 31372 185903 4.75% 0.825% 13 42.346 4051 4063 4073 rBV4 25494 169589 4.33% 0.753% 14 44.990 4339 4351 4367 rBV3 17035 145041 3.71% 0.644%

Sum of corrected areas: 22532703 LB.D GCMS0531.M Tue Jun 04 09:04:50 2002

NYC-WTC_000015044

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NYC-WTC_000015044Source: NYC Law Department, mirrored locally

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