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GCMS analysis results for sample AE12675, June 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12675 conducted on June 6, 2002.

NYC-WTC_000015016–000015026

Folder label: “GCMS X 5/30/02 A 6/1/02

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NYC 9/11 Public Portal Document LSC Area Percent Report . Data File C: \HPCHEM\ 1 \DATA\MAY3102\12675.D Vial: 20 Acq On 1 Jun 2002 6:41 am Operator:. Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.058 325 328 331 rBV 44728 89821 2.39% 0.431% 2 8.113 331 334 345 rVB 24661 65003 1.73% 0.312% 3 12.070 759 765 785 rBV 1069941 2717625 72.19% 13.044% 4 15.696 1153 1160 1176 rBV 1683072 3669130 97.47% 17.611% 5 20.993 1730 1737 1753 rBV 1772270 3764417 100.00% 18.068% 6 23.132 1961 1970 1978 rBV 961679 2045591 54.34% 9.818% 7 25.427 2213 2220 2231 rBV2 1765933 3738365 99.31% 17.943% 8 25.574 2231 2236 2244 rVB 14438 43096 . 1.14% 0.207% 9 33.478 3089 3097 3110 rBV2 1143480 2699743 71.72% 12.958% 10 37.655 3544 3552 3566 rBV2 691342 2001808 53.18% 9.608%

Sum of corrected areas: 20834599 12675.D GCMS0531.M Mon Jun 03 11:45:19 2002

NYC-WTC_000015021

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NYC-WTC_000015021Source: NYC Law Department, mirrored locally

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