GCMS analysis results for sample AE12162, June 2002

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Library Search Compound Report Data File C:\HPCHEM\l\DATA\MAY3102\12162.D Vial: 16 Acq On 1 Jun 2002 2:45 am Operator: Morgan Sample re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531 .M (RTE Integrator) += Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Decanedioic acid, bis(2-ethylh Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

35.99 260.07 ug/1 14738100 Perylene-d12 37.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual (D ecanedioicacid, bis (2 -ethylhexyl 426 C26H50O4 000122-62-3(87 2 Nonane, 4-methyl—- " 142 C10H22 017301-94-9 27 3 [1,1’-Biphenyl]-4-ol, 3-amino- 185 C12H11NO• 001134-36-7 27 4 2-Undecene, 4,5-dimethyl-, [R@,S@-( 182 C13H26 055170-93-9 25 Abundance Scan 3371 (35.991 min): 12162.D (-) m/z 185.10 100.00% 185

57 5000 112 — 83

miz—> 34 , "pundmir Tr 4n 143 166 204 240T268 —mmup 297316—umnn 1 ■ i‘ “11 “ ‘ ■ i ■ 340 —369 20 40 60 80 100120140160180200220240260280300320340360380400420 397—mn—426 —Bpmnm m—mm 35.60 35.80 36.00 36.20 36.40 m/z 57.00 56.75% Abundance #55661: Decanedioic acid, bis(2-ethylhexyl) ester 185

5000 57 -p-T ‘ I ‘ ‘

112 35.60 35.80 36.00 36.20 36.40 m/z 70.05 41.78% 83 143 166 298 ' i" ■ ■ i‘ •P * “ i nfmmmpmmm miz—> 20 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #66223: Nonane, 4-methyl- 57

35.60 35,80.36.00 36.20 36.40 5000 m/z 71.05 41.47%

27 98 11 | J , 142 m/z—> 20 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #19199: [1,1-Biphenyl]-4-ol, 3-amino- 185 35.60 35.80 36.00 36.20 36.40 m/z 43.00 31.34%

5000 156

miz—> rZCuL TTT 20 40 60 80 100120140160180200220240260280300320340360380400420 ................................................ 35.60 35.80 36.00 36.20 36.40

12162.D GCMS0531.M Mon Jun 03 11:44:42 2002 Page 1

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