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GCMS blank analysis report sample AE12094, June 2002

Machine-extracted title · confidence 95%

Laboratory blank report for GCMS analysis of volatile organic compounds conducted on May 31, 2002.

NYC-WTC_000014956–000014963

Folder label: “GCMS X 5/30/02 A 6/1/02

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NYC 9/11 Public Portal Document LSC Area Percent Report . Data File : C:\HPCHEM\1\DATA\MAY3102\LBA.D Vial: 13 Acq On : 31 May 2002 11:48 pm Operator: Morgan Sample : gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.062 325 329 344 rBV 40865 102680 2.65% 0.489% 2 12.064 760 765 779 rBV 1141400 2686522 69.39% 12.798% 3 15.690 1154 1160 1178 rBV 1692100 3672218 94.85% 17.494% 4 20.987 1730 1737 1753 rBV 1744410 3794377 98.01% 18.076% 5 23.136 1960 1971 1983 rBV 850870 1875444 48.44% 8.934% 6 25.431 2213 2221 2232 rBV2 1743361 3871472 100.00% 18.443% 7 33.473 3090 3097 3113 rBV2 1220027 2856143 73.77% 13.606% 8 37.659 3545 3553 3568 rBV2 724757 2132570 55.08% 10.159%

Sum of corrected areas: 20991426 LBA.D GCMS0531.M Mon Jun 03 11:45:57 2002

NYC-WTC_000014960

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NYC-WTC_000014960Source: NYC Law Department, mirrored locally

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