Reference standard report for GCMS analysis of volatile organic compounds conducted on May 30-31, 2002.
NYC-WTC_000014754–000014763Folder label: “GCMS X 5/29/02 A 5/30/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAY3002\12093.D Vial: 13 Acq On : 31 May 2002 1:52 am Operator: Morgan Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 31 11:25 2002 Quant Results File :,GCMS0520 .RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) A A Title : 209 625/TCLP calibration table UN Last Update : Mon May 20 15:10:30 2002 PW ' Response via : Initial Calibration AAO DataAcq Meth : GCMS0528 - /W
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.06 152 599881 40.00 ug/1 -0.08 10) Naphthalene-d8 15.69 136 2419349 40.00 ug/1 -0.10 17) Acenaphthene-dl0 21.00 164 1140557 40.00 ug/1 -0.09 30) Phenanthrene-diO 25.43 188 1772863 40.00 ug/1 -0.10 38) Chrysene-dl2 33.47 240 1080809 40.00 ug/1 -0.13 44) Perylene-dl2 37.66 264 689518 40.00 ug/1 -0.14 System Monitoring Compounds 28) TCMX 23.14 209 204210 35.62 ug/L -0.10 Spiked Amount 40.000 Recovery 89.05% Target Compounds Qvalue 2) N-nitrosodimethylamine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 12.06 146 360 N.D. 5) 1,4-Dichlorobenzene 12.06 146 360 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.75 128 144 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.35 165 100 N.D. 25) Diethylphthalate 22.48 149 1798 N.D. 26) 4-Chlorophenylphenylether 23.14 204 1489 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzene 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.14 168 773 N.D. 32) 4-Bromophenylphenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 3 4) Phenanthrene 25.49 178 351 N.D. (#) = qualifier out of range (m) = manual integration 12093.D GCMS0520.M Fri May 31 11:25:32 2002 Page 1
NYC-WTC_000014756
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NYC-WTC_000014843
GCMS laboratory analysis report for sample AE12097 showing unknown compounds and surrogate recovery data from June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014771
Calibration table data for GCMS analysis including internal standards and response factors from May 31, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014825
Calibration table and internal standard data for sample AE12095 analyzed on May 31, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014807
Calibration data for sample AE11284 analyzed using Method 508 on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014976
GCMS laboratory analysis report for sample AE12094 showing unknown compounds and surrogate recovery data from June 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014987
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE12162 conducted on June 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013351
Analytical report for sample AE12154 detailing GCMS results and surrogate recovery data from June 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013387
Laboratory report documenting GCMS analysis of sample AE12158 conducted on June 7, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013360
Analytical report for sample AE12155 detailing GCMS results and surrogate recovery data from June 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013342
Analytical report for sample AE12153 detailing GCMS results and surrogate recovery data from June 6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013762
Report documenting analysis for unknown compounds and surrogate recovery in sample AE12284.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013864
Gas chromatography-mass spectrometry analysis of sample AE12223 conducted on June 3, 2002, detecting unknown compounds and 2,4-DDD surrogate at 76% recovery.
1 shared topics · Same agency, volume and box · similarity 0.996
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NYC-WTC_000014729
Laboratory report documenting GCMS analysis of sample AE12574 conducted on June 7, 2002, including surrogate recovery data.
Filed in the same folder
NYC-WTC_000014730
Header page from a GCMS method document covering the period of May 29 to May 30, 2002.
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NYC-WTC_000014733
GCMS blank analysis report for sample AE12093 dated 05/31/2002 showing all measured organic compounds below minimum reporting limits (MRL) of 2.0 micrograms.
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NYC-WTC_000014742
Laboratory blank report for GCMS analysis of volatile organic compounds conducted on May 31, 2002.
Filed in the same folder
NYC-WTC_000014746
Calibration results for gas chromatography mass spectrometry analysis of volatile organic compounds from May 31, 2002.
Filed in the same folder