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GCMS analysis results for sample AE12539, June 2002

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Laboratory report documenting GCMS analysis of sample AE12539 conducted on June 7, 2002, including surrogate recovery data.

NYC-WTC_000014670–000014679

Folder label: “GCMS X 5/28/02 A 6/4/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\JUNO3 02\12539.D Vial: 20 Acq On 4 Jun 2002 3:56 am Operator: Sample gc/ms scan 5/28 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jun 4 11:45 2002 Quant Results File: GCMS0531.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 31 09:43:55 2002 Response via : Initial Calibration DataAcq Meth : GCMS0531

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.42 178 388 N.D. 36) Di-n-butylphthalate 27.41 149 25150 0.50 ug/1 97 3 7) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.47 228 1869 N.D. 42) Bis(2-ethylhexyl)phthalate 33.71 149 2071 N.D. 43) Chrysene 33.47 228 1869 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 4 6) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.65 252 1866 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo (g,h, Dperylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 12539.D GCMS0531.M Tue Jun 04 11:46:11 2002 Page 2

NYC-WTC_000014673

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NYC-WTC_000014673Source: NYC Law Department, mirrored locally

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