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GCMS analysis results, sample AE12533, June 2002

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Laboratory report showing GCMS analysis results for sample AE12533 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014552–000014577

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\l\DATA\052902\12533.D Vial: 24 Acq On : 30 May 2002 4:49 am Operator: McLean Sample : gc/ms scan 5/28 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator), Title : 508 Modified GC/MS scan Signal : TIC peak R.T. first max last PK peak. corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.479 64 68 92 PV 7 8000 279040 0.59% 0.110% 2 3.720 92 109 ill PV 3 25074 1001616 2.11% 0.396% 3 3.761 111 116 119 W 4 25887 731865 1.54% 0.289% 4 3.790 119 121 123 W 3 24047 276940 0.58% 0.109% 5 3.814 123 125 129 W 5 23647 538727 1.13% 0.213% 6 3.849 129 131 138 W 5 23242 651852 1.37% 0.258% 7 3.908 138 141 145 W 4 21283 539154 1.13% 0.213% 8 3.949 145 148 153 W 4 19890 498691 1.05% 0.197% 9 3.990 153 155 169 W 9 19412 997751 2.10% 0.394% 10 4.125 174 178 186 W 9 16240 648654. 1.36% 0.256% 11 4.295 205 207 212 W 4 12718 292938 0.62% 0.116% 12 4.337 212 214 218 W 5 12626 199715 0.42% 0.079% 13 4.536 240 248 257 W 9 12586 575664 1.21% 0.228% 14 5.100 342 344 346 W 2 3656 37221 0.08% 0.015% 15 5.371 385 390 397 W 8 3885 92675 0.19% 0.037% 16 5.911 479 482 484 PV 3 1757 15769 0.03% 0.006% 17 5.946 484 488 503 W 26379 694686 1.46% 0.275% 18 9.895 1147 1160 1182 PV 1585614 31560031 66.37% 12.477% 19 12.374 1571 1582 1592 PV 28333 451320 0.95% 0.178% 20 13.391 1744 1755 1771 PV 2345029 42627655 89.65% 16.853% 21 13.544 1775 1781 1790 W 7099 128682 0.27% 0.051% 22 15.653 2130 2140 2145 W 3 1701 32668 0.07% 0.013% 23 16.705 2310 2319 2322 PV 3 3849 59586 0.13% 0.024% 24 16.734 2322 2324 2332 W 4 2459 44998 0.09% 0.018% 25 17.110 2383 2388 2394 W 4 6179 94062 0.20% 0.037% 26 17.621 2466 2475 2480 W 3 2838 47212 0.10% 0.019% 27 18.526 2615 2629 2658 PV 2454638 47037479 98.92% 18.596% 28 20.101 2893 2897 2904 W 3 3888 67733 0.14% 0.027% 29 20.506 2954 2966 2975 PV 1228024 22959410 . 48.28% 9.077% 30 21.352 3096 3110 3117 PV 2 9602 163798 0.34% 0.065% 31 22.533 3305 3311 3319 W 3 16934 316769 0.67% 0.125% 32 22.909 3365 3375 3395 PV 2 2300611 47551049 100.00% 18.799% 33 23.068 3395 3402 3418 W 19765 395898 0.83% 0.157% 34 25.048 3729 3739 3758 W 19059 390179 0.82% 0.154% 35 30.759 4699 4711 4750 PV 2 1413020 31561940 66.37% 12.478% 36 30.994 4750 4751 4753 W 2 3660 31886 0.07% 0.013% 37 31.018 4753 4755 4760 W 4 3396 68207 0.14% 0.027% 12533.D 052202.M Mon Jun 03 11:45:15 2002 Page 1

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NYC-WTC_000014557Source: NYC Law Department, mirrored locally

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